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Superior Activity of Isomorphously Substituted MOFs with MIL-100(M=Al, Cr, Fe, In, Sc, V) Structure in the Prins Reaction: Impact of Metal Type

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388955%3A_____%2F17%3A00473610" target="_blank" >RIV/61388955:_____/17:00473610 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216208:11310/17:10368341

  • Result on the web

    <a href="http://dx.doi.org/10.1002/cplu.201600456" target="_blank" >http://dx.doi.org/10.1002/cplu.201600456</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1002/cplu.201600456" target="_blank" >10.1002/cplu.201600456</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Superior Activity of Isomorphously Substituted MOFs with MIL-100(M=Al, Cr, Fe, In, Sc, V) Structure in the Prins Reaction: Impact of Metal Type

  • Original language description

    The catalytic behavior of isomorphously substituted MIL-100(M) (M=Al, Cr, Fe, In, Sc, V) is investigated for the synthesis of nopol through the Prins condensation ofpinene with paraformaldehyde. The large mesoporous cages of the metal-organic frameworks provide a sustainable confinement for the formation of the target product (100% selectivity for nopol over all materials studied). MIL-100(Sc) and MIL-100(V) exhibit the highest yields (up to 90%) of nopol after just 20min from the beginning of the reaction, owing to their high concentrations of accessible Lewis sites possessing intermediate acidity. The high catalytic activity (reaching almost 90%pinene conversion) even upon decreasing the amount of catalyst from 100 to 25mg (0.025 and 0.0063g(catalyst)mmol(substrate)(-1), respectively), the stability of its structure, and the possibility to use it several times, make MIL-100(V) a promising material for applications in acid-catalyzed reactions under mild reaction conditions.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10403 - Physical chemistry

Result continuities

  • Project

    <a href="/en/project/GA14-07101S" target="_blank" >GA14-07101S: Combined Experimental and Theoretical Investigation of Catalytic Properties of Metal Organic Frameworks</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2017

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    ChemPlusChem

  • ISSN

    2192-6506

  • e-ISSN

  • Volume of the periodical

    82

  • Issue of the periodical within the volume

    1

  • Country of publishing house

    DE - GERMANY

  • Number of pages

    8

  • Pages from-to

    152-159

  • UT code for WoS article

    000394182400014

  • EID of the result in the Scopus database

    2-s2.0-84995378019