Optimization of a Flow Rate for a Hyphenation of Voltammetry with Electrospray Ionization Mass Spectrometry

Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388963%3A_____%2F12%3A00384357" target="_blank" >RIV/61388963:_____/12:00384357 - isvavai.cz</a>
Alternative codes found
RIV/61388955:_____/12:00384357
Result on the web
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DOI - Digital Object Identifier
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Result language
angličtina
Original language name
Optimization of a Flow Rate for a Hyphenation of Voltammetry with Electrospray Ionization Mass Spectrometry
Original language description
The hyphenation of an electrochemical cell prior to mass spectrometer with electrospray ionization allows studying of products and/or of intermediates of electrode reactions. The measurement is realized in a flowing system. The flow rate of the sample markedly influences the MS signal intensity of the product. The calculated optimum value for the electrochemical cell with the sweep volume 0.72 ?L is in the range from 0.4 to 0.5 mL h -1 . The experimental optimal value is 0.45 mL h -1 . The optimizationof the flow rate has to be provided individually for each product, because the intensity also depends on the rate of the electrode reaction and product stability.
Czech name
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Czech description
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Project
Result was created during the realization of more than one project. More information in the Projects tab.
Continuities
I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Publication year
2012
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Article name in the collection
XXXII. Moderní elektrochemické metody. Sborník přednášek
ISBN
978-80-905221-0-7
ISSN
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e-ISSN
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Number of pages
4
Pages from-to
54-57
Publisher name
BEST servis
Place of publication
Ústí nad Labem
Event location
Jetřichovice
Event date
May 21, 2012
Type of event by nationality
EUR - Evropská akce
UT code for WoS article
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