Evaluation of an ion source with a tubular nebulizer for microflow atmospheric pressure chemical ionization
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388963%3A_____%2F18%3A00490859" target="_blank" >RIV/61388963:_____/18:00490859 - isvavai.cz</a>
Alternative codes found
RIV/00216208:11310/18:10391624
Result on the web
<a href="http://dx.doi.org/10.1007/s00706-018-2172-4" target="_blank" >http://dx.doi.org/10.1007/s00706-018-2172-4</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1007/s00706-018-2172-4" target="_blank" >10.1007/s00706-018-2172-4</a>
Alternative languages
Result language
angličtina
Original language name
Evaluation of an ion source with a tubular nebulizer for microflow atmospheric pressure chemical ionization
Original language description
An atmospheric pressure chemical ionization (APCI) source designed for microliter-per-minute flow rates (0.5-10.0 mm(3)/min) was constructed. A simple resistively heated 1/8 in. OD tube-based nebulizer, together with a corona-discharge electrode was positioned in front of the entrance capillary of a mass spectrometer. Working parameters of the ion source were optimized, and its performance was evaluated. The limit of detection for directly infused acridine was found to be lower for micro-APCI (10 fmol/s) than for conventional APCI (170 fmol/s), and the linear dynamic range was significantly wider for the micro-APCI source. The micro-APCI and conventional APCI sources provided similar, but not identical mass spectra. The micro-APCI source was used as a detector for high-performance liquid chromatography at 10 mm(3)/min, the limit of detection for acridine was 690 fmol, which was about ten times lower value than in conventional HPLC.
Czech name
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Czech description
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Classification
Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
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OECD FORD branch
10406 - Analytical chemistry
Result continuities
Project
<a href="/en/project/GA16-01639S" target="_blank" >GA16-01639S: Micro- and nanoflow atmospheric pressure ionizations for bioanalytical mass spectrometry</a><br>
Continuities
P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)
Others
Publication year
2018
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Monatshefte fur Chemie
ISSN
0026-9247
e-ISSN
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Volume of the periodical
149
Issue of the periodical within the volume
6
Country of publishing house
AT - AUSTRIA
Number of pages
8
Pages from-to
987-994
UT code for WoS article
000433333300001
EID of the result in the Scopus database
2-s2.0-85042070102