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pH and Medium Polarity-Induced Self-Assembly of Fmoc-Tryptophan into Multiple Superstructures: An Experimental and Theoretical Investigations

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388963%3A_____%2F25%3A00636153" target="_blank" >RIV/61388963:_____/25:00636153 - isvavai.cz</a>

  • Result on the web

    <a href="https://doi.org/10.1002/cplu.202500036" target="_blank" >https://doi.org/10.1002/cplu.202500036</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1002/cplu.202500036" target="_blank" >10.1002/cplu.202500036</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    pH and Medium Polarity-Induced Self-Assembly of Fmoc-Tryptophan into Multiple Superstructures: An Experimental and Theoretical Investigations

  • Original language description

    Self-assembly of functionalized molecular building blocks is an effective and resource-saving bottom-up technique to generate multiple superstructures with various functionality and morphologies. The nature of the molecule and the factors controlling the overall self-assembly process are extremely vital in fundamental aspects of self-assembly, which deliver insights into the fabrication of multiple assemblies with specific functionality. The self-assembly of suitably functionalized amino acids leads to the formation of diverse structures with distinct properties, making them ideal bio-organic scaffolds for various applications. The present study reports, the pH and solvent polarity-induced self-assembly of 9-fluorenylmethoxycarbonyl (Fmoc)-Tryptophan into various self-assembled superstructures with morphological individualities, explore the plausible pathway of morphological transformation of Fmoc-Trp into multiple superstructures having a wide range of well-defined morphologies, including spheres, hollow spheres, nanoflowers, nanosheets, nanorods, and cube-like structures, as characterized through conventional microscopic techniques. Detailed UV-vis, fluorescence, powder X-ray diffraction analysis, and Fourier transform infrared analyses reveal significant insights into the intermolecular interactions, which trigger the overall self-assembly process. The computational studies, including full geometry optimization and molecular dynamics simulations, are conducted to investigate the aggregation properties of modified amino acids (Fmoc-Trp). These studies highlight the crucial role of pi-pi stacking and hydrogen bonding in tuning the overall self-assembly with morphological variation.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10403 - Physical chemistry

Result continuities

  • Project

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2025

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    ChemPlusChem

  • ISSN

    2192-6506

  • e-ISSN

    2192-6506

  • Volume of the periodical

    90

  • Issue of the periodical within the volume

    6

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    12

  • Pages from-to

    e202500036

  • UT code for WoS article

    001461336400001

  • EID of the result in the Scopus database

    2-s2.0-105002169770