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Stability of the sodium content in selected botanical reference materials

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61389005%3A_____%2F18%3A00501267" target="_blank" >RIV/61389005:_____/18:00501267 - isvavai.cz</a>

  • Alternative codes found

    RIV/67985831:_____/18:00501267

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Stability of the sodium content in selected botanical reference materials

  • Original language description

    Sodium mass fractions in NIST standard reference materials (SRM) SRM 1547 Peach Leaves and SRM 1515 Apple leaves determined by INAA in our laboratory in recent years has been higher than the certified values. Similarly, increased values were published for SRM 1547 by several other laboratories. The increased Na mass fractions was found also for freshly opened SRM 1547 bottle and for material originating from a different lab. Increased Na mass fractions were confirmed by ICP-MS analysis of both materials. Analysis of archived samples revealed that sodium mass fraction in materials stored in polyethylene capsules is in agreement with the certified values. The sodium content in the glass of SRM 1547 bottle was roughly 10 %. Direct measurement of the Na depth profile by micro-PIXE was not indicative whether Na is released, i.g., by a glass corrosion due to residual humidity in the botanical material. However, a model experiment with freshly prepared and pulverized peach leaves demonstrated that such a scenario is possible for leaf-based materials. Although the study was focused on two NIST materials, the process is possible for any material with rather low Na content.

  • Czech name

  • Czech description

Classification

  • Type

    D - Article in proceedings

  • CEP classification

  • OECD FORD branch

    10406 - Analytical chemistry

Result continuities

  • Project

    <a href="/en/project/GBP108%2F12%2FG108" target="_blank" >GBP108/12/G108: Preparation, modification and characterization of materials by radiation</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2018

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Article name in the collection

    Sborník přednášek 7. ročníku Referenční materiály a mezilaboratorní porovnávání zkoušek

  • ISBN

    978-80-86380-98-8

  • ISSN

  • e-ISSN

  • Number of pages

    7

  • Pages from-to

    65-71

  • Publisher name

    2THETA

  • Place of publication

    Lednice

  • Event location

    Lednice

  • Event date

    Nov 5, 2018

  • Type of event by nationality

    EUR - Evropská akce

  • UT code for WoS article