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Polyaniline: Aniline oxidation with strong and weak oxidants under various acidity

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61389013%3A_____%2F17%3A00473613" target="_blank" >RIV/61389013:_____/17:00473613 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216208:11320/17:10367412

  • Result on the web

    <a href="http://dx.doi.org/10.1016/j.matchemphys.2017.03.028" target="_blank" >http://dx.doi.org/10.1016/j.matchemphys.2017.03.028</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.matchemphys.2017.03.028" target="_blank" >10.1016/j.matchemphys.2017.03.028</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Polyaniline: Aniline oxidation with strong and weak oxidants under various acidity

  • Original language description

    Aniline was oxidized with three strong inorganic oxidants (ammonium peroxydisulfate, cerium(IV) sulfate, potassium dichromate), two weak inorganic oxidants (iron(III) chloride, silver nitrate), and one organic oxidant (p-benzoquinone) in aqueous solutions of methanesulfonic acid (MSA) of various concentration. Whereas oxidation of aniline with ammonium peroxydisulfate yielded high-molecular-weight conducting polyaniline (PANI) in the whole acidity range, the oxidation with cerium(IV) sulfate led also to a single product close to PANI with considerably lower molecular weight and lower conductivity. Potassium dichromate gave PANI only at high concentration of MSA. The use of iron(III) chloride yielded composite mixtures of PANI and low-molecular-weight aniline oligomers. The oxidation of aniline with silver nitrate led to composites of silver and an organic part, which was constituted either by aniline oligomers or conducting polyaniline or both. p-Benzoquinone as oxidant produced mainly aniline oligomers with poor conductivity and 2,5-dianilino-p-benzoquinone-like structure detected in FTIR and Raman spectra when oxidation proceeded with weak oxidants. A general model of oxidation with strong and weak oxidants was formulated.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10404 - Polymer science

Result continuities

  • Project

    <a href="/en/project/GA16-02787S" target="_blank" >GA16-02787S: Conducting polymer cryogels</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2017

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Materials Chemistry and Physics

  • ISSN

    0254-0584

  • e-ISSN

  • Volume of the periodical

    194

  • Issue of the periodical within the volume

    15 June

  • Country of publishing house

    CH - SWITZERLAND

  • Number of pages

    13

  • Pages from-to

    206-218

  • UT code for WoS article

    000401385400026

  • EID of the result in the Scopus database

    2-s2.0-85018525523