Underivatized amylose and cellulose as new stationary phases for hydrophilic interaction chromatography
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61989592%3A15310%2F13%3A33147304" target="_blank" >RIV/61989592:15310/13:33147304 - isvavai.cz</a>
Alternative codes found
RIV/61388971:_____/13:00425776
Result on the web
<a href="http://dx.doi.org/10.1002/jssc.201300577" target="_blank" >http://dx.doi.org/10.1002/jssc.201300577</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1002/jssc.201300577" target="_blank" >10.1002/jssc.201300577</a>
Alternative languages
Result language
angličtina
Original language name
Underivatized amylose and cellulose as new stationary phases for hydrophilic interaction chromatography
Original language description
Two polysaccharide stationary phases have been newly suggested for application in hydrophilic interaction chromatography (HILIC). Both columns (amylose-silica, 250 x 4.6 mm, 5 m and cellulose-silica, 250 x 4.6 mm, 5 m) demonstrated a satisfactory retention of polar compounds. The influence of the mobile-phase composition (acetonitrile content, pH, salt concentration) on the retention was in agreement with the HILIC concept. The phases showed a very similar behavior, typical efficiency of about 50000 plates/m, cellulose retained test compounds somewhat more strongly. Under the experimental conditions, electrostatic (non-HILIC-type) interactions due to the dissociation of silanol groups on the silica surface did not influence the retention, noticeably. The applicability of polysaccharide stationary phases for the chromatography of polar compounds was proven by the separation of mixtures of sugars (fructose, glucose, saccharose, maltose, trehalose) or vitamins (nicotinamide, pyridoxine, r
Czech name
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Czech description
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Classification
Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
CB - Analytical chemistry, separation
OECD FORD branch
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Result continuities
Project
<a href="/en/project/ED2.1.00%2F03.0058" target="_blank" >ED2.1.00/03.0058: Regional Centre of Advanced Technologies and Materials</a><br>
Continuities
P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>S - Specificky vyzkum na vysokych skolach
Others
Publication year
2013
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Journal of Separation Science
ISSN
1615-9306
e-ISSN
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Volume of the periodical
36
Issue of the periodical within the volume
20
Country of publishing house
DE - GERMANY
Number of pages
6
Pages from-to
3345-3350
UT code for WoS article
000325482500006
EID of the result in the Scopus database
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