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Controlled nucleation of crystallization process as an efficient tool to tune the properties of corticosteroid API

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61989592%3A15310%2F22%3A73612814" target="_blank" >RIV/61989592:15310/22:73612814 - isvavai.cz</a>

  • Alternative codes found

    RIV/61989592:15640/22:73612814

  • Result on the web

    <a href="https://www.sciencedirect.com/science/article/pii/S0032591022002285" target="_blank" >https://www.sciencedirect.com/science/article/pii/S0032591022002285</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.powtec.2022.117334" target="_blank" >10.1016/j.powtec.2022.117334</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Controlled nucleation of crystallization process as an efficient tool to tune the properties of corticosteroid API

  • Original language description

    Crystallization as one of the final steps in the industrial production of active pharmaceutical ingredients (APIs) significantly influences their physicochemical and rheological properties. Different crystallization procedures including antisolvent crystallization, seeding crystallization, crystallization with templates and sonocrystallization were utilized for the production of corticosteroid APIs-fluticasone propionate. The final crystalline APIs obtained by individual crystallization procedures were characterized by a wide range of characterization techniques. We show that nucleation is a critical step that significantly affects APIs&apos; properties. Controlled nucleation thus represents an easy method for managing these properties. Well-designed nucleation yields to crystalline products, which does not necessitate any post-processing including, e.g., micronization. These findings can be widely applied to the production of API with targeted properties.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10403 - Physical chemistry

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2022

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    POWDER TECHNOLOGY

  • ISSN

    0032-5910

  • e-ISSN

    1873-328X

  • Volume of the periodical

    402

  • Issue of the periodical within the volume

    APR

  • Country of publishing house

    CH - SWITZERLAND

  • Number of pages

    8

  • Pages from-to

    "17334-1"-117334

  • UT code for WoS article

    000793463500010

  • EID of the result in the Scopus database

    2-s2.0-85128166241