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Mössbauer Study on the Conversion of Different Iron-Based Catalysts Used in Carbon Nanotube Synthesis

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61989592%3A15310%2F23%3A73620806" target="_blank" >RIV/61989592:15310/23:73620806 - isvavai.cz</a>

  • Result on the web

    <a href="https://www.mdpi.com/2079-4991/13/23/3010" target="_blank" >https://www.mdpi.com/2079-4991/13/23/3010</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.3390/nano13233010" target="_blank" >10.3390/nano13233010</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Mössbauer Study on the Conversion of Different Iron-Based Catalysts Used in Carbon Nanotube Synthesis

  • Original language description

    The phase composition and comparison of iron-based catalysts used for the synthesis of carbon nanotubes were investigated. This work reflects typical catalyst conditions and their evolution during the growth of carbon nanotubes. The preparation of carbon nanotubes was carried out by chemical vapour deposition at temperatures between 800 and 1100 °C. Ferrocene or zero-valent iron nanoparticles were used as “catalysts”, and toluene, ferrocene and the ferrocene–toluene solution played the role of carbon precursors, respectively. The phase composition of the prepared product was studied by Mössbauer spectroscopy and X-ray powder diffraction. Mössbauer analysis was particularly useful for samples with a low content of the nanoparticle form of the catalyst. The composition of the prepared samples differed depending on the synthesis temperature, catalyst and precursor. Phase analysis revealed the presence of α-Fe and Fe3C in all samples. In addition, γ-Fe and iron oxides were identified under certain conditions. Scanning and transmission electron microscopy confirmed the carbon nanotube/nanofibre-like morphology and the presence of iron species.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    21001 - Nano-materials (production and properties)

Result continuities

  • Project

    <a href="/en/project/TN02000069" target="_blank" >TN02000069: National centre of competence for Materials, Advanced Technologies, Coatings and their Applications</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2023

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Nanomaterials

  • ISSN

    2079-4991

  • e-ISSN

    2079-4991

  • Volume of the periodical

    13

  • Issue of the periodical within the volume

    23

  • Country of publishing house

    CH - SWITZERLAND

  • Number of pages

    15

  • Pages from-to

    "3010-1"-"3010-15"

  • UT code for WoS article

    001118001000001

  • EID of the result in the Scopus database

    2-s2.0-85178959238