Separation of a mixture of luteolin-7-rutinoside and luteolin-7-neohesperidoside isolated from Ligustrum vulgare L.
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F62157124%3A16370%2F09%3A00002093" target="_blank" >RIV/62157124:16370/09:00002093 - isvavai.cz</a>
Result on the web
—
DOI - Digital Object Identifier
—
Alternative languages
Result language
angličtina
Original language name
Separation of a mixture of luteolin-7-rutinoside and luteolin-7-neohesperidoside isolated from Ligustrum vulgare L.
Original language description
Simple and rapid TLC and column chromatographic methods have been established for separation of luteolin-7-rutinoside and luteolin-7-neohesperidoside on polyamide. A flavonoid mixture was isolated from the butanolic fraction of a methanolic extract of leaves of Ligustrum vulgare L. HPLC analysis of the isolated mixture showed the presence of two compounds in a ratio of approximately 1:1. TLC and column separation was achieved on polyamide with CHCl 3 -MeOH-2-butanone-acetylacetone 9:4:2:1 as mobile phase. After successful separation, the isolated compounds were identified by UV, MS, and NMR spectroscopy and by acid hydrolysis then comparison with authentic samples. Luteolin-7-neohesperidoside was isolated from Ligustrum vulgare L. for the first time.
Czech name
—
Czech description
—
Classification
Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
FR - Pharmacology and apothecary chemistry
OECD FORD branch
—
Result continuities
Project
—
Continuities
S - Specificky vyzkum na vysokych skolach
Others
Publication year
2009
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Journal of Planar Chromatography, modern TLC
ISSN
0933-4173
e-ISSN
—
Volume of the periodical
22
Issue of the periodical within the volume
4
Country of publishing house
HU - HUNGARY
Number of pages
4
Pages from-to
—
UT code for WoS article
000269552900012
EID of the result in the Scopus database
—