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Protein Structure-sensitive Analysis by Normal Pulse Voltammetry

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68081707%3A_____%2F16%3A00471946" target="_blank" >RIV/68081707:_____/16:00471946 - isvavai.cz</a>

  • Result on the web

    <a href="http://dx.doi.org/10.1002/elan.201600202" target="_blank" >http://dx.doi.org/10.1002/elan.201600202</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1002/elan.201600202" target="_blank" >10.1002/elan.201600202</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Protein Structure-sensitive Analysis by Normal Pulse Voltammetry

  • Original language description

    Earlier we showed that constant current chronopotentiometric stripping (CPS) at mercury-containing electrodes reflects changes in proteins, such as denaturation, single amino acid exchange or protein damage by physical and chemical agents. Here we attempted to compare performance of the galvanostatic CPS with the potentiostatic normal pulse voltammetry (NPV). We have found that repeated 50ms or longer NPV pulses denature the surface-attached protein. Using shorter pulses and adapting other NPV settings we have been able to obtain a good resolution of native (folded) and denatured (unfolded) bovine serum albumin. On the other hand, partial denaturation of the surface-attached native bovine serum albumin during the potential scanning may prevent detection of small conformational changes in the protein.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    BO - Biophysics

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/GA15-15479S" target="_blank" >GA15-15479S: New tools for research and diagnostics of diseases. Microfluidic reactors and electrochemistry for analysis of proteins and their glycosylation.</a><br>

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2016

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Electroanalysis

  • ISSN

    1040-0397

  • e-ISSN

  • Volume of the periodical

    28

  • Issue of the periodical within the volume

    11

  • Country of publishing house

    DE - GERMANY

  • Number of pages

    6

  • Pages from-to

    2884-2889

  • UT code for WoS article

    000387891400034

  • EID of the result in the Scopus database