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Synthesis, characterization and crystal structure of N,N'-Bis(2,3-Dimethoxybenzylidene)-1,2-Diaminoethane

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378271%3A_____%2F11%3A00369331" target="_blank" >RIV/68378271:_____/11:00369331 - isvavai.cz</a>

  • Result on the web

    <a href="http://dx.doi.org/10.1007/s10870-011-9988-7" target="_blank" >http://dx.doi.org/10.1007/s10870-011-9988-7</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1007/s10870-011-9988-7" target="_blank" >10.1007/s10870-011-9988-7</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Synthesis, characterization and crystal structure of N,N'-Bis(2,3-Dimethoxybenzylidene)-1,2-Diaminoethane

  • Original language description

    Synthesis and characterization of single crystals of a new organic Schiff-base derivative, N,N'-bis(2,3-dimethoxybenzylidene)-1,2-diaminoethane is reported. Good quality single crystals with size 10 mm x 1 mm x 1 mm were grown by slow evaporation technique from a methanol solution at room temperature. The grown crystals have been characterized by elemental analyses and functional groups were identified using FT-IR and 1H-NMR spectroscopy. Crystal structure of the title compound has been determined by single crystal X-ray diffraction. The title compound has a monoclinic symmetry, space group P21/c, lattice parameters are a = 4.4159(3) A, b = 14.2333(9) A, c = 15.0601(10) A, beta = 97.755(5)°, Z = 2, V = 937.91(11) A3.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    BM - Solid-state physics and magnetism

  • OECD FORD branch

Result continuities

  • Project

  • Continuities

    Z - Vyzkumny zamer (s odkazem do CEZ)

Others

  • Publication year

    2011

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Journal of Chemical Crystallography

  • ISSN

    1074-1542

  • e-ISSN

  • Volume of the periodical

    41

  • Issue of the periodical within the volume

    12

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    6

  • Pages from-to

    1955-1960

  • UT code for WoS article

    000296883100025

  • EID of the result in the Scopus database