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A low-cost, environment-friendly and solvent-free route for synthesis of AgBr nanoparticles

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378271%3A_____%2F15%3A00448310" target="_blank" >RIV/68378271:_____/15:00448310 - isvavai.cz</a>

  • Result on the web

    <a href="http://dx.doi.org/10.1016/j.spmi.2015.01.030" target="_blank" >http://dx.doi.org/10.1016/j.spmi.2015.01.030</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.spmi.2015.01.030" target="_blank" >10.1016/j.spmi.2015.01.030</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    A low-cost, environment-friendly and solvent-free route for synthesis of AgBr nanoparticles

  • Original language description

    We report on the synthesis of AgBr nanoparticles average size below 20 nm by from AgNO3 and a thiosemicarbazone ligand, Brcatsc [Brcatsc = 2-bromo-3-phenylpropenalthiosemicarbazone]. Brcatsc was prepared by reacting ?-bromocinnam-aldehyde and thiosemicarbazide (1:1, molar ratio) in hot ethanol characterized by elemental analyses (CHN), FT-IR, 1H NMR spectroscopy and single crystal X-ray diffraction. AgBr nanoparticles were prepared by heating the mixture of AgNO3 and Brcatsc at 600 C for 3 h under aerobic condition, and characterized by X-ray powder diffraction (XRD), scanning electron microsco py (SEM) and transmission electron microscopy (TEM). The XRD pattern clearly indicates the formation of AgBr nanoparticles while SEM and TEM results reveal their uniformity and purity.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    BM - Solid-state physics and magnetism

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/GA14-03276S" target="_blank" >GA14-03276S: Aspherical effects and their application for statistically correct crystal structure analysis</a><br>

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2015

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Superlattices and Microstructures

  • ISSN

    0749-6036

  • e-ISSN

  • Volume of the periodical

    82

  • Issue of the periodical within the volume

    Jun

  • Country of publishing house

    GB - UNITED KINGDOM

  • Number of pages

    8

  • Pages from-to

    18-25

  • UT code for WoS article

    000357141400003

  • EID of the result in the Scopus database

    2-s2.0-84923819897