A low-cost, environment-friendly and solvent-free route for synthesis of AgBr nanoparticles
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378271%3A_____%2F15%3A00448310" target="_blank" >RIV/68378271:_____/15:00448310 - isvavai.cz</a>
Result on the web
<a href="http://dx.doi.org/10.1016/j.spmi.2015.01.030" target="_blank" >http://dx.doi.org/10.1016/j.spmi.2015.01.030</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1016/j.spmi.2015.01.030" target="_blank" >10.1016/j.spmi.2015.01.030</a>
Alternative languages
Result language
angličtina
Original language name
A low-cost, environment-friendly and solvent-free route for synthesis of AgBr nanoparticles
Original language description
We report on the synthesis of AgBr nanoparticles average size below 20 nm by from AgNO3 and a thiosemicarbazone ligand, Brcatsc [Brcatsc = 2-bromo-3-phenylpropenalthiosemicarbazone]. Brcatsc was prepared by reacting ?-bromocinnam-aldehyde and thiosemicarbazide (1:1, molar ratio) in hot ethanol characterized by elemental analyses (CHN), FT-IR, 1H NMR spectroscopy and single crystal X-ray diffraction. AgBr nanoparticles were prepared by heating the mixture of AgNO3 and Brcatsc at 600 C for 3 h under aerobic condition, and characterized by X-ray powder diffraction (XRD), scanning electron microsco py (SEM) and transmission electron microscopy (TEM). The XRD pattern clearly indicates the formation of AgBr nanoparticles while SEM and TEM results reveal their uniformity and purity.
Czech name
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Czech description
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Classification
Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
BM - Solid-state physics and magnetism
OECD FORD branch
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Result continuities
Project
<a href="/en/project/GA14-03276S" target="_blank" >GA14-03276S: Aspherical effects and their application for statistically correct crystal structure analysis</a><br>
Continuities
I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace
Others
Publication year
2015
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Superlattices and Microstructures
ISSN
0749-6036
e-ISSN
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Volume of the periodical
82
Issue of the periodical within the volume
Jun
Country of publishing house
GB - UNITED KINGDOM
Number of pages
8
Pages from-to
18-25
UT code for WoS article
000357141400003
EID of the result in the Scopus database
2-s2.0-84923819897