A simple cryotransfer method for 3D electron diffraction measurements of highly sensitive samples

Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378271%3A_____%2F25%3A00637059" target="_blank" >RIV/68378271:_____/25:00637059 - isvavai.cz</a>
Result on the web
<a href="https://hdl.handle.net/11104/0368313" target="_blank" >https://hdl.handle.net/11104/0368313</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1107/S1600576725002456" target="_blank" >10.1107/S1600576725002456</a>

Result language
angličtina
Original language name
A simple cryotransfer method for 3D electron diffraction measurements of highly sensitive samples
Original language description
The accurate characterization of highly sensitive materials using 3D electron diffraction (3D ED) is often challenged by sample degradation caused by exposure to moisture, air, temperature variations and high vacuum during the transfer and introduction into the transmission electron microscope (TEM). A cryogenic sample-transfer protocol is presented here, designed to enable the safe and effective transfer of reactive samples into the TEM, ensuring an inert and moisture-free environment throughout the process. The protocol was validated by redetermining the crystal structures of the moisture-sensitive, strongly oxidizing and highly reactive compounds XeF2, XeF4 and XeF2·XeF4 cocrystal.
Czech name
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Czech description
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Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
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OECD FORD branch
10302 - Condensed matter physics (including formerly solid state physics, supercond.)

Project
Result was created during the realization of more than one project. More information in the Projects tab.
Continuities
I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Publication year
2025
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

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