Preparation of Water-Soluble Fullerene Derivative by Reaction with Peracetic Acid and Its nanoparticles Size Distribution

Result code in IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F70565813%3A_____%2F12%3A%230000288" target="_blank" >RIV/70565813:_____/12:#0000288 - isvavai.cz</a>

Result on the web

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DOI - Digital Object Identifier

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Result language

angličtina

Original language name

Preparation of Water-Soluble Fullerene Derivative by Reaction with Peracetic Acid and Its nanoparticles Size Distribution

Original language description

A water-soluble C60 fullerene Derivative (DF) was obtained by reaction of C60 fullerene with peracetic acid and subsequent hydrolysis.The DF water-solution of the concentration of 147 +-0,1 mg/L at ambient temperature and neutral pH remains stable for along time without the mechanical action (settling) and coagulation of particles. The concentration and the sice of nanoparticles i DFwarer solution were analysed by the NanoSight KM10HSB. Even this system contained a larger particles an analysis after filtration by 0,1 um filter and under 20 x and 10 x objective showed a nice and quite monodispersed distribution of modal particle size 42+53 and 60 nm in concentration 3,5 x 10-8 particles/mL respectively.Comparison of pristine C60 and DF by transmissionelectron microscopy TEM (100kV) and scannig election microscopy SEMresults showed differences in the size of the irregular complexes and in their crystallinity. Fourier transformed infrared (FTIR) spcterometry of DF detected -OH groups, a

Czech name

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Czech description

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Type

J_x - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

CEP classification

CB - Analytical chemistry, separation

OECD FORD branch

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Project

<a href="/en/project/VG20102014049" target="_blank" >VG20102014049: Research of the possibilities for application of a new materials (focusing on nano-materials) and advanced technologies for protection of people against the exposure to CBRN materials, with emphasis on critical infrastructure</a><br>

Continuities

P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Publication year

2012

Confidentiality

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Name of the periodical

Journal of Materials Science and Engineering A

ISSN

2161-6213

e-ISSN

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Volume of the periodical

2

Issue of the periodical within the volume

1

Country of publishing house

US - UNITED STATES

Number of pages

12

Pages from-to

86-97

UT code for WoS article

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EID of the result in the Scopus database

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