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Selected Spectrometric Metrods for Determination of Iodine in Biological Samples

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F70883521%3A28160%2F22%3A63557380" target="_blank" >RIV/70883521:28160/22:63557380 - isvavai.cz</a>

  • Alternative codes found

    RIV/70883521:28110/22:63557380

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Selected Spectrometric Metrods for Determination of Iodine in Biological Samples

  • Original language description

    This article compares different methods for determination of iodine in biological samples. Most frequently, indirect methods are applied in clinical practice. Sandell-Kolthoff spectrophotometric method of iodine determination [1] ranks among the most widely used ones; researchers also developed other modifications of the above method. Regarding direct determination, the following methods are considered the most suitable ones: emission spectrometry with inductively coupled plasma (ICP-OES), electrochemical methods, mass spectrometry with inductively coupled plasma (ICP-MS), and nuclear activation analysis (NAA) [2]. The ICP-MS and NAA are costly, but iodine can be analyzed directly regardless of its form, oxidation state, and isotopic distribution of iodine [3]. On the contrary, electrochemical, and ICP-OES determinations can be complicated with remarkable spectral interferences and also with dependence on possible presence of various forms and oxidation states of iodine in samples [4].We compared three most frequently used methods for determination of iodine in selected biological materials: Sandell-Kolthoff spectrophotometric determination, ICP-OES and ICP-MS techniques [5]. The samples of biological materials such as foods and food supplements corresponding to content of iodine in urine were selected (Jooste and Strydom 2010). A NIST-SRM-1549 Milk powder certified reference material (CRM) with certified iodine concentration (3.38+0.6 mg/kg) was used to control the accuracy of the total iodine determination. The least accurate results were obtained by ICP-OES in analyses of given CRM (5.64+0.39 mg/kg), better results were acquired by spectrophotometric method (4.53+0.23 mg/kg) and the most accurate results were provided by ICP-MS method (3.36+0.12 mg/kg of iodine).

  • Czech name

  • Czech description

Classification

  • Type

    O - Miscellaneous

  • CEP classification

  • OECD FORD branch

    21101 - Food and beverages

Result continuities

  • Project

    <a href="/en/project/ED2.1.00%2F03.0111" target="_blank" >ED2.1.00/03.0111: Centre of Polymer Systems</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2022

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů