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Voltammetric and amperometric determination of metoclopramide on boron-doped diamond film electrode

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11310%2F12%3A10125455" target="_blank" >RIV/00216208:11310/12:10125455 - isvavai.cz</a>

  • Result on the web

    <a href="http://dx.doi.org/10.2478/s11532-012-0056-8" target="_blank" >http://dx.doi.org/10.2478/s11532-012-0056-8</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.2478/s11532-012-0056-8" target="_blank" >10.2478/s11532-012-0056-8</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Voltammetric and amperometric determination of metoclopramide on boron-doped diamond film electrode

  • Original language description

    New methods for the determination of metoclopramide, antiemetic and gastroprokinetic pharmaceutical, were developed, using differential pulse voltammetry (DPV) and flow injection analysis (FIA) with amperometric detection on a boron-doped diamond film electrode. Electrode pretreatment necessary to ensure the stable results was investigated and it was found, that while DPV requires frequent electrode cleaning, FIA with a sufficiently high flow rate can maintain a stable signal with no signs of electrodepassivation. The calculated quantification limits of the DPV and FIA with amperometric detection were 0.13 mu mol L-1 and 0.015 mmol L-1, respectively. The applicability of the new methods was verified by the determination of metoclopramide in a pharmaceutical preparation. FIA with amperometic detection proved to be sensitive, accurate and, due to the resistance of the electrode to the passivation, also simple to handle.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CG - Electrochemistry

  • OECD FORD branch

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>Z - Vyzkumny zamer (s odkazem do CEZ)<br>S - Specificky vyzkum na vysokych skolach<br>I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2012

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Central European Journal of Chemistry

  • ISSN

    1895-1066

  • e-ISSN

  • Volume of the periodical

    10

  • Issue of the periodical within the volume

    4

  • Country of publishing house

    PL - POLAND

  • Number of pages

    8

  • Pages from-to

    1310-1317

  • UT code for WoS article

    000304618900035

  • EID of the result in the Scopus database