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The Lithiation Reactivity and Selectivity of Differentially Branched Alkyldiphenylphosphine Oxides - A Simple and Versatile Approach to ortho-Functionalized Arylphosphine Oxides

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11310%2F15%3A10294428" target="_blank" >RIV/00216208:11310/15:10294428 - isvavai.cz</a>

  • Alternative codes found

    RIV/61388963:_____/15:00443900

  • Result on the web

    <a href="http://dx.doi.org/10.1002/adsc.201400861" target="_blank" >http://dx.doi.org/10.1002/adsc.201400861</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1002/adsc.201400861" target="_blank" >10.1002/adsc.201400861</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    The Lithiation Reactivity and Selectivity of Differentially Branched Alkyldiphenylphosphine Oxides - A Simple and Versatile Approach to ortho-Functionalized Arylphosphine Oxides

  • Original language description

    Alkyldiphenylphosphine oxides typically undergo alpha-deprotonation with alkyllithium reagents. Here, the lithiation of differentially branched alkyl-diphenylphosphine oxides was investigated and a diverse, but predictable reactivity was found. gamma-Branched derivatives undergo selective directed ortho-metalation (DoM) using butyllithium and TMEDA as an additive. With decreasing degree of gamma-branching alpha-lithiation becomes predominant. The ortho-phosphinoyllithium intermediates are subject to functionalization and C-C bond forming reactions, thus providing a convenient approach to new phosphine oxides and phosphine-borane complexes, which have a good potential for an approach to new ligands for catalysis.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CC - Organic chemistry

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/GAP207%2F11%2F1598" target="_blank" >GAP207/11/1598: A New Carbanion Rearrangement and Its Application in Organic Synthesis</a><br>

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2015

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Advanced Synthesis and Catalysis

  • ISSN

    1615-4150

  • e-ISSN

  • Volume of the periodical

    357

  • Issue of the periodical within the volume

    4

  • Country of publishing house

    DE - GERMANY

  • Number of pages

    7

  • Pages from-to

    793-799

  • UT code for WoS article

    000351222700021

  • EID of the result in the Scopus database

    2-s2.0-84923869873