Synthesis, NMR and X-ray characterisation of 6-substituted 4-amino-5-aryldiazenyl-1-arylpyridazinium salts
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216275%3A25310%2F05%3A00003064" target="_blank" >RIV/00216275:25310/05:00003064 - isvavai.cz</a>
Result on the web
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DOI - Digital Object Identifier
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Alternative languages
Result language
angličtina
Original language name
Synthesis, NMR and X-ray characterisation of 6-substituted 4-amino-5-aryldiazenyl-1-arylpyridazinium salts
Original language description
A new simple method has been used to prepare 6-substituted 4-(subst. amino)-5-aryldiazenyl-l-arylpyridazinium salts from N-methyl- or N-aryl-3-amino-l-phenylbut-2-en-l-ones and 4-aminopent-3-en-2-ones and substituted benzenediazonium tetrafluoroborates or hexafluorophosphates. The structure of selected derivatives was studied by means of 15N NMR spectra and X-ray.
Czech name
Syntéza, NMR a X-ray charakterizace 4-amino-6-substituovaných-5-aryldiazenyl-1-arylpyridaziniových solí
Czech description
Novou jednoduchou metodikou byly z N-methyl-, resp. N-aryl 3-amino-1-fenylbut-2-en-1-onů, resp. 4-aminopent-3-en-2-onů a substituovaných benzendiazonium-tetrafluoroborátů, resp. hexafluorofosfátů připraveny 4-amino-6-substituované-5-aryldiazenyl-1-arylpyridaziniové soli. Připravené sloučeniny byly charakterizovány pomocí 1H a 13C NMR spekter. U vybraných derivátů byla struktura studována i pomocí 15N NMR spekter a X-ray.
Classification
Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
CC - Organic chemistry
OECD FORD branch
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Result continuities
Project
<a href="/en/project/GA203%2F03%2F0356" target="_blank" >GA203/03/0356: Tautomerism and hydrogen bonding in beta-eneminone derivatives. Multinuclear and X-ray study</a><br>
Continuities
Z - Vyzkumny zamer (s odkazem do CEZ)
Others
Publication year
2005
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Tetrahedron
ISSN
0040?4020
e-ISSN
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Volume of the periodical
61
Issue of the periodical within the volume
34
Country of publishing house
CZ - CZECH REPUBLIC
Number of pages
8
Pages from-to
8130-8137
UT code for WoS article
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EID of the result in the Scopus database
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