Development of Solid-Phase Extraction and HPLC/MS Methods for Deoxynivalenol Determination in Barley and Malt

Result code in IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F44555601%3A13440%2F09%3A00004845" target="_blank" >RIV/44555601:13440/09:00004845 - isvavai.cz</a>

Result on the web

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DOI - Digital Object Identifier

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Result language

angličtina

Original language name

Development of Solid-Phase Extraction and HPLC/MS Methods for Deoxynivalenol Determination in Barley and Malt

Original language description

A method for determination of deoxynivalenol (DON) in cereals has been developed and applied. Solid phase extraction with Envicarb clean-up columns and subsequent separation by HPLC-MS on LUNA C18(2) column were used. DON was detected by MS detector in positive mode. The developed method is relatively cheap and fast with high sensitivity. The method was used for determination of the deoxynivalenol content in barley and malt. Detection limit for is for barley (malt) is 25 mg/kg (30 mg/kg). A variation inquantity of DON in samples after a malting process was observed.

Czech name

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Czech description

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Type

J_x - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

CEP classification

CB - Analytical chemistry, separation

OECD FORD branch

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Project

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Continuities

S - Specificky vyzkum na vysokych skolach

Publication year

2009

Confidentiality

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Name of the periodical

Chemické listy

ISSN

0009-2770

e-ISSN

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Volume of the periodical

103

Issue of the periodical within the volume

8

Country of publishing house

CZ - CZECH REPUBLIC

Number of pages

5

Pages from-to

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UT code for WoS article

000269243500009

EID of the result in the Scopus database

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