Development of a fast UHPLC-MS/MS for the analysis of selected priority micropollutants in wastewater samples

Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60460709%3A41330%2F19%3A79758" target="_blank" >RIV/60460709:41330/19:79758 - isvavai.cz</a>
Result on the web
<a href="https://www.tandfonline.com/doi/full/10.1080/03067319.2019.1660874" target="_blank" >https://www.tandfonline.com/doi/full/10.1080/03067319.2019.1660874</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1080/03067319.2019.1660874" target="_blank" >10.1080/03067319.2019.1660874</a>

Result language
angličtina
Original language name
Development of a fast UHPLC-MS/MS for the analysis of selected priority micropollutants in wastewater samples
Original language description
In recent years, there have been many reports on the presence of organic compounds in different compartments of the aquatic environment. The subject of our research was the development of a new method for the determination of selected organic micropollutants and their transformation products in wastewater samples. A rapid and sensitive ultra-high performance liquid chromatographic method coupled with tandem mass spectrometry has been developed and used for the separation and determination of 1H-benzotriazole, imidacloprid and clarithromycin in wastewater samples. The analytes were separated on a ZORBAX SB-C3 column with a gradient elution within 3,0 min. The analytes were isolated from wastewater samples by solid-phase extraction. Extraction was carried out on the Oasis HLB cartridges and methanol:acetone (1:1, v/v) was used for elution. The working ranges of the developed method were 1-100 ng L-1. The recovery ranged from 62% to 102% and intra- and inter-day precision was lower than 13% for all anal
Czech name
—
Czech description
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Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
—
OECD FORD branch
10406 - Analytical chemistry

Publication year
2019
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Name of the periodical
International Journal of Environmental Analytical Chemistry
ISSN
0306-7319
e-ISSN
1029-0397
Volume of the periodical
2019
Issue of the periodical within the volume
N
Country of publishing house
GB - UNITED KINGDOM
Number of pages
20
Pages from-to
1-20
UT code for WoS article
000485959600001
EID of the result in the Scopus database
2-s2.0-85072046649

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