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Influence of non-ideal behavior on esterification kinetics modeling

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22310%2F20%3A43920698" target="_blank" >RIV/60461373:22310/20:43920698 - isvavai.cz</a>

  • Result on the web

    <a href="https://link.springer.com/article/10.1007%2Fs11144-020-01796-7" target="_blank" >https://link.springer.com/article/10.1007%2Fs11144-020-01796-7</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1007/s11144-020-01796-7" target="_blank" >10.1007/s11144-020-01796-7</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Influence of non-ideal behavior on esterification kinetics modeling

  • Original language description

    The well-known kinetics of Fischer esterification has already been reported for various systems. Despite this fact, the kinetic model of esterification of oleic acid and methanol under catalysis with sulfuric acid is still debated in the literature. The main reason is the two-phase character of the reaction mixture being neglected in kinetic studies. Contrary to this, the kinetics of autocatalytic esterification of cyclic alcohols with formic acid have not been published so far. Here, we present a kinetic study of both systems to assess the influence of the non-ideal (multi-phase) behavior on kinetic modeling. For the system of autocatalytic esterification of cyclic alcohols, we have found that a simple kinetic model without activity coefficients provides a good description of the experimental data. However, the same model is insufficient for the system of oleic acid and methanol. Therefore, we have developed a new approach based on kinetic modeling, including activity coefficients. Consequently, we have been able to describe for the first time the kinetics of oleic acid esterification in a homogeneous reaction mixture. Moreover, we provide a novel explanation for the commonly observed inhibition of this reaction by water as a result of phase equilibria in the reaction mixture.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10403 - Physical chemistry

Result continuities

  • Project

  • Continuities

    S - Specificky vyzkum na vysokych skolach

Others

  • Publication year

    2020

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Reaction Kinetics Mechanisms and Catalysis

  • ISSN

    1878-5190

  • e-ISSN

  • Volume of the periodical

    130

  • Issue of the periodical within the volume

    2

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    16

  • Pages from-to

    617-632

  • UT code for WoS article

    000539924100003

  • EID of the result in the Scopus database