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Potential of Liquid Chromatography - Atmospheric Pressure Chemical Ionisation Tandem Mass Spectrometry for Determination of Fosetyl-aluminium Residues in Dried Hops

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22330%2F04%3A00013122" target="_blank" >RIV/60461373:22330/04:00013122 - isvavai.cz</a>

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Potential of Liquid Chromatography - Atmospheric Pressure Chemical Ionisation Tandem Mass Spectrometry for Determination of Fosetyl-aluminium Residues in Dried Hops

  • Original language description

    New analytical procedure for the determination of fosetyl-aluminium in hop cones (also called "hops") was developed. Liquid chromatography-atmospheric pressure chemical ionisation tandem mass spectrometry (LC-APCIMS/MS) allowed a highly selective determination of this fungicide which facilitated the sample preparation. The sufficiently low detection limit (1 mg/kg of dried hops) with the acceptable method performance characteristics (RSD 9%, recovery 76% - at the level of 10 mg/kg) complies with the need to inspect the observance of maximal residual limit 100 mg/kg. The application of LC-MS technique thus provided an effective way of fosetyl-aluminium determination in the complex hops matrix.

  • Czech name

    Možnosti kapalinové chromatografie-tandemové hmotnostní spektrometrie s chemickou ionizací za atmosférického tlaku při stanovení reziduí fosetyl-aluminia v sušených chmelových šišticích

  • Czech description

    Možnosti kapalinové chromatografie-tandemové hmotnostní spektrometrie s chemickou ionizací za atmosférického tlaku při stanovení reziduí fosetyl-aluminia v sušených chmelových šišticích

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    GM - Food industry

  • OECD FORD branch

Result continuities

  • Project

  • Continuities

    Z - Vyzkumny zamer (s odkazem do CEZ)

Others

  • Publication year

    2004

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Czech Journal of Food Science

  • ISSN

    1212-1800

  • e-ISSN

  • Volume of the periodical

    22

  • Issue of the periodical within the volume

    1

  • Country of publishing house

    CZ - CZECH REPUBLIC

  • Number of pages

    5

  • Pages from-to

    24-28

  • UT code for WoS article

  • EID of the result in the Scopus database