Analysis of MCPD and Glycidyl Fatty Acid Esters in Refined Plant Oils by Supercritical Fluid ChromatographyHigh-Resolution Mass Spectrometry
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22330%2F22%3A43925030" target="_blank" >RIV/60461373:22330/22:43925030 - isvavai.cz</a>
Result on the web
—
DOI - Digital Object Identifier
—
Alternative languages
Result language
angličtina
Original language name
Analysis of MCPD and Glycidyl Fatty Acid Esters in Refined Plant Oils by Supercritical Fluid ChromatographyHigh-Resolution Mass Spectrometry
Original language description
2- and 3-chloropropane-1,2-diol (2- and 3-MCPD) and their fatty acid esters (2- and 3-MCPDE) together with glycidyl fatty acids esters (GE) belong to a group of process-induced contaminants. They are formed in high temperature environments and most commonly occur in refined vegetable oils. With regards to the documented toxicity of free 3-MCPD (IARC group 2B) and glycidol (IARC group 2A), since 2021 maximum limits for GE and 3-MCPDE are enforceable in the European Union. Hence, the requirements for adequate analytical methods is constantly increasing.The aim of this study was to develop a method enabling a rapid, simultaneous determination of 9 3-MCPDE and 7 GE in vegetable oils and fats, with the use of supercritical fluid chromatography coupled with mass spectrometry (SFC-MS). Contrary to a routine GC-MS method the sample throughput was greatly increased. The recovery, repeatability and limits of quantification required by legislation were met for majority of analytes.
Czech name
—
Czech description
—
Classification
Type
J<sub>ost</sub> - Miscellaneous article in a specialist periodical
CEP classification
—
OECD FORD branch
10406 - Analytical chemistry
Result continuities
Project
Result was created during the realization of more than one project. More information in the Projects tab.
Continuities
P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)
Others
Publication year
2022
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
LC GC Europe
ISSN
1471-6577
e-ISSN
—
Volume of the periodical
35
Issue of the periodical within the volume
s7
Country of publishing house
US - UNITED STATES
Number of pages
7
Pages from-to
28-34
UT code for WoS article
—
EID of the result in the Scopus database
—