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Electrochemical oxidation of anti-inflammatory drug meloxicam and its determination using boron doped diamond electrode

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61989592%3A15310%2F20%3A73603855" target="_blank" >RIV/61989592:15310/20:73603855 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216275:25310/20:39916369

  • Result on the web

    <a href="https://www.sciencedirect.com/science/article/pii/S1572665719310264" target="_blank" >https://www.sciencedirect.com/science/article/pii/S1572665719310264</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.jelechem.2019.113758" target="_blank" >10.1016/j.jelechem.2019.113758</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Electrochemical oxidation of anti-inflammatory drug meloxicam and its determination using boron doped diamond electrode

  • Original language description

    Voltammetric behavior of a nonsteroidal anti-inflammatory drug meloxicam was firstly studied using boron doped diamond electrode (BDDE). Two irreversible anodic current peaks were observed in wide pH range at potentials +900 mV and +1400 mV vs. saturated silver-silver chloride electrode. Mechanism of the electrochemical oxidation was proposed and confirmed using high performance liquid chromatography/mass spectrometry analysis of electrolyzed meloxicam solutions. Subsequently, an analytical method for meloxicam determination was developed using differential pulse voltammetry in connection with BDDE. This method provides low limit of detection (5.9 x 10(-8) mol L-1) and wide linear dynamic range (2.5 x 10(-7)-8.5 x 10(-5) mol L-1). Finally, model solutions as well as pharmaceutical preparations were successfully analyzed, and the meloxicam content was determined.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10406 - Analytical chemistry

Result continuities

  • Project

    <a href="/en/project/GA17-03868S" target="_blank" >GA17-03868S: New Methods of Electrochemical Monitoring of Biologically Active Organic Compounds in Environmental, Biological and Food Matrices</a><br>

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2020

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    JOURNAL OF ELECTROANALYTICAL CHEMISTRY

  • ISSN

    1572-6657

  • e-ISSN

  • Volume of the periodical

    858

  • Issue of the periodical within the volume

    FEB

  • Country of publishing house

    CH - SWITZERLAND

  • Number of pages

    9

  • Pages from-to

    "113758-1"-"113758-9"

  • UT code for WoS article

    000515205600004

  • EID of the result in the Scopus database

    2-s2.0-85076893090