Synthesis of new cobalt(III) Schiff base complex: a new precursor for preparation Co3O4 nanoparticles via solid-state thermal decomposition

Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378271%3A_____%2F14%3A00435001" target="_blank" >RIV/68378271:_____/14:00435001 - isvavai.cz</a>
Result on the web
<a href="http://dx.doi.org/10.1016/j.molstruc.2014.04.043" target="_blank" >http://dx.doi.org/10.1016/j.molstruc.2014.04.043</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1016/j.molstruc.2014.04.043" target="_blank" >10.1016/j.molstruc.2014.04.043</a>

Result language
angličtina
Original language name
Synthesis of new cobalt(III) Schiff base complex: a new precursor for preparation Co3O4 nanoparticles via solid-state thermal decomposition
Original language description
A new mononuclear octahedral cobalt(III) Schiff base complex has been synthesized and characterized by elemental analyses (CHN) and FT-IR spectroscopy and used as precursor for preparation of Co3O4 nanoparticles. The crystal structure of this compound has been determined by single-crystal X-ray diffraction. The coordination sphere about cobalt(III) ion consists of three phenolato oxygens and three imino nitrogen atoms from three Schiff base ligands, thus forming a distorted octahedral geometry. Each Schiff base ligand acts as a chelate using phenolato oxygen and imino nitrogen. Subsequently, pure phase Co3O4 nanoparticles, with an average size in the range 10?20 nm, were obtained by solid-state thermal decomposition of the synthesized complex at 450 degC under air atmosphere for 3 h.
Czech name
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Czech description
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Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
BM - Solid-state physics and magnetism
OECD FORD branch
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Project
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Continuities
I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Publication year
2014
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

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