Synthesis and crystal structure of [Pb(gly)2]n New lead(II) coordination polymer with glycine ligand

Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378271%3A_____%2F19%3A00519691" target="_blank" >RIV/68378271:_____/19:00519691 - isvavai.cz</a>
Result on the web
<a href="https://doi.org/10.22052/JNS.2019.01.02" target="_blank" >https://doi.org/10.22052/JNS.2019.01.02</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.22052/JNS.2019.01.02" target="_blank" >10.22052/JNS.2019.01.02</a>

Result language
angličtina
Original language name
Synthesis and crystal structure of [Pb(gly)2]n New lead(II) coordination polymer with glycine ligand
Original language description
The [Pb(gly)2]n (1) have been synthesized and characterized by elemental analyses, IR, 1H NMR and 13C NMR spectroscopy. The single crystal structure of 1 show the complex is 2D coordination polymer with octahedral environment that is formed into 3D supramolecule through hydrogen bond. Structural determination of compound 1 reveals the Pb(II) ion is four coordinated, bonded to a nitrogen, oxygen and two carbon atoms from the Glycine ligand. PbO nanoparticles were synthesized by calcinations of compound 1 at 500, 550 and 600 °C under air atmosphere. The PbO nanostructure was characterized by scanning electron microscopy and X-ray powder diffraction. The thermal stability of compound 1 was studied by thermal gravimetric and differential thermal analyses.
Czech name
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Czech description
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Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
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OECD FORD branch
10302 - Condensed matter physics (including formerly solid state physics, supercond.)

Project
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Continuities
I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Publication year
2019
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

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