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The critical influence of surface topography on nanoindentation measurements of a-SiC: H films

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68407700%3A21220%2F15%3A00233625" target="_blank" >RIV/68407700:21220/15:00233625 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216305:26310/15:PU115699

  • Result on the web

    <a href="http://dx.doi.org/10.1016/j.surfcoat.2014.11.049" target="_blank" >http://dx.doi.org/10.1016/j.surfcoat.2014.11.049</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.surfcoat.2014.11.049" target="_blank" >10.1016/j.surfcoat.2014.11.049</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    The critical influence of surface topography on nanoindentation measurements of a-SiC: H films

  • Original language description

    Hydrogenated amorphous silicon-carbon films were prepared on polished silicon wafers from a tetravinylsilane precursor via plasma-enhanced chemical vapor deposition. The grain structure was developed at the film surface using high powers (50-70. W), as observed by atomic force microscopy (AFM). Conventional and cyclic nanoindentation measurements revealed different mechanical responses for indentation into and outside of the selected isolated grain with a spherical cap geometry with a radius greater than that of the indenter (50. nm). The finite element method was employed to simulate the behavior of the grain under deformation by an indenter to correctly interpret the nanoindentation data. Scanning probe measurements using modulus mapping (dynamic mechanical analysis) and atomic force acoustic microscopy confirmed that the surface topography had a critical influence on the determined mechanical properties, which were significantly underestimated. Our experimental and simulation study demonstrates that nanoindentation and scanning probe measurements must be performed on strictly flat surfaces. This conclusion applies to all AFM measurements performed in contact and semi-contact mode used to characterize mechanical properties based on the geometry of the contact.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CF - Physical chemistry and theoretical chemistry

  • OECD FORD branch

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2015

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Surface & Coatings Technology

  • ISSN

    0257-8972

  • e-ISSN

  • Volume of the periodical

    261

  • Issue of the periodical within the volume

    leden

  • Country of publishing house

    NL - THE KINGDOM OF THE NETHERLANDS

  • Number of pages

    8

  • Pages from-to

    114-121

  • UT code for WoS article

    000348255500015

  • EID of the result in the Scopus database

    2-s2.0-84920733588