Optimization of Liquid Jet System for Laser-Induced Breakdown Spectroscopy Analysis

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216224%3A14740%2F16%3A00089403" target="_blank" >RIV/00216224:14740/16:00089403 - isvavai.cz</a>

Výsledek na webu

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DOI - Digital Object Identifier

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Jazyk výsledku

angličtina

Název v původním jazyce

Optimization of Liquid Jet System for Laser-Induced Breakdown Spectroscopy Analysis

Popis výsledku v původním jazyce

Laser-induced breakdown spectroscopy (LIBS) enables direct in-situ analysis of samples in any state of matter. This capability of LIBS enables its utilization in vast variety of applications, for instance bioapplications and online monitoring. We report on the optimization of a system for direct elemental analysis of samples in liquid phase using LIBS technique. This system consists of a peristaltic pump and a thin specially designed nozzle producing a thin flow of liquid solution/suspension. Such arrangement was used to reduce splashes of liquid and sedimentation of suspension and thus to improve the repeatability of an experiment. Firstly, stepping frequency of the peristaltic pump was synchronized with a flash lamp of ablation laser source. Using such synchronization, changes in pressure and hence volume of liquid along the step of the peristaltic pump were mitigated. Changes in the liquid flow volume affect the laser ablation process in the sense of so-called effective volume function.

Název v anglickém jazyce

Optimization of Liquid Jet System for Laser-Induced Breakdown Spectroscopy Analysis

Popis výsledku anglicky

Laser-induced breakdown spectroscopy (LIBS) enables direct in-situ analysis of samples in any state of matter. This capability of LIBS enables its utilization in vast variety of applications, for instance bioapplications and online monitoring. We report on the optimization of a system for direct elemental analysis of samples in liquid phase using LIBS technique. This system consists of a peristaltic pump and a thin specially designed nozzle producing a thin flow of liquid solution/suspension. Such arrangement was used to reduce splashes of liquid and sedimentation of suspension and thus to improve the repeatability of an experiment. Firstly, stepping frequency of the peristaltic pump was synchronized with a flash lamp of ablation laser source. Using such synchronization, changes in pressure and hence volume of liquid along the step of the peristaltic pump were mitigated. Changes in the liquid flow volume affect the laser ablation process in the sense of so-called effective volume function.

Druh

O - Ostatní výsledky

CEP obor

CB - Analytická chemie, separace

OECD FORD obor

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Projekt

<a href="/cs/project/ED1.1.00%2F02.0068" target="_blank" >ED1.1.00/02.0068: CEITEC - central european institute of technology</a><br>

Návaznosti

P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Rok uplatnění

2016

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů