Morphology study of 2-ethylhexyl acrylate/cellulose acetate propionate microcapsules prepared via solvent evaporation technique

Kód výsledku v IS VaVaI

RIV/00216305:26310/17:PU124424 - isvavai.cz

Výsledek na webu

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DOI - Digital Object Identifier

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Jazyk výsledku

angličtina

Název v původním jazyce

Morphology study of 2-ethylhexyl acrylate/cellulose acetate propionate microcapsules prepared via solvent evaporation technique

Popis výsledku v původním jazyce

Novel 2-ethylhexyl acrylate (2-EHA)/cellulose acetate propionate (CAP) microcapsules with mononuclear core-shell morphology are potentially an interesting model system for polymerization inside microcapsules. Microencapsulation was performed by solvent evaporation technique from dichloromethane solution dispersed in poly(vinyl alcohol) solution. Microcapsule morphology, which evolved from partially raspberry-like to a bowl like due to premature shell formation and subsequent solvent evaporation, was captured by microscopy imaging techniques. Thus it has been concluded that kinetics of CAP shell formation play a crucial role in preparation of 2 EHA/CAP microcapsules. Moreover, microcapsules were ruptured in compression under microscope in order to evaluate fracture type. Ductile fracture of microcapsule shell was observed. Shell thickness of 0.3 μm was estimated by scanning electron microscopy. Even though bowl-like morphology of microcapsules was not favorable for polymerization inside microcapsules,

Název v anglickém jazyce

Morphology study of 2-ethylhexyl acrylate/cellulose acetate propionate microcapsules prepared via solvent evaporation technique

Popis výsledku anglicky

Novel 2-ethylhexyl acrylate (2-EHA)/cellulose acetate propionate (CAP) microcapsules with mononuclear core-shell morphology are potentially an interesting model system for polymerization inside microcapsules. Microencapsulation was performed by solvent evaporation technique from dichloromethane solution dispersed in poly(vinyl alcohol) solution. Microcapsule morphology, which evolved from partially raspberry-like to a bowl like due to premature shell formation and subsequent solvent evaporation, was captured by microscopy imaging techniques. Thus it has been concluded that kinetics of CAP shell formation play a crucial role in preparation of 2 EHA/CAP microcapsules. Moreover, microcapsules were ruptured in compression under microscope in order to evaluate fracture type. Ductile fracture of microcapsule shell was observed. Shell thickness of 0.3 μm was estimated by scanning electron microscopy. Even though bowl-like morphology of microcapsules was not favorable for polymerization inside microcapsules,

Druh

O - Ostatní výsledky

CEP obor

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OECD FORD obor

10404 - Polymer science

Projekt

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Návaznosti

S - Specificky vyzkum na vysokych skolach

Rok uplatnění

2017

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů