Sequential Extraction of Organic Fractions from Biochar using Eluotropic Series of Organic Solvents

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216305%3A26310%2F21%3APU143849" target="_blank" >RIV/00216305:26310/21:PU143849 - isvavai.cz</a>

Výsledek na webu

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DOI - Digital Object Identifier

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Jazyk výsledku

angličtina

Název v původním jazyce

Sequential Extraction of Organic Fractions from Biochar using Eluotropic Series of Organic Solvents

Popis výsledku v původním jazyce

In this work, we performed a sequential chemical extraction with a series of organic solvents with an increasing polarity (trichloromethane – TCM1 < ethyl acetate – EAC2 < acetone – ACE3 < acetonitrile – ACN4 < n-propanol – PRO5 < methanol – MET6) on Czech biochar and subjected the obtained organic fractions to a physicochemical characterization utilizing thermal and spectrometric methods of structural and compositional analysis. Spectrometric techniques such as Ultraviolet-visible (UV/Vis) and Attenuated Total Reflectance (ATR-FTIR) were combined with thermogravimetric and elemental analysis of the organic fractions. Biochar was homogenized and 5000 mg was then inserted in a thimble, and Soxhlet sequential extracted for 24–168 h. The organic fractions isolated from the biochar were concentrated using a rotary evaporator. Furthermore, the brown to black extracts were dried in a vacuum desiccator filled with anhydrous sodium sulphate as a drying medium. In total, the fractionation procedure extracted o

Název v anglickém jazyce

Sequential Extraction of Organic Fractions from Biochar using Eluotropic Series of Organic Solvents

Popis výsledku anglicky

In this work, we performed a sequential chemical extraction with a series of organic solvents with an increasing polarity (trichloromethane – TCM1 < ethyl acetate – EAC2 < acetone – ACE3 < acetonitrile – ACN4 < n-propanol – PRO5 < methanol – MET6) on Czech biochar and subjected the obtained organic fractions to a physicochemical characterization utilizing thermal and spectrometric methods of structural and compositional analysis. Spectrometric techniques such as Ultraviolet-visible (UV/Vis) and Attenuated Total Reflectance (ATR-FTIR) were combined with thermogravimetric and elemental analysis of the organic fractions. Biochar was homogenized and 5000 mg was then inserted in a thimble, and Soxhlet sequential extracted for 24–168 h. The organic fractions isolated from the biochar were concentrated using a rotary evaporator. Furthermore, the brown to black extracts were dried in a vacuum desiccator filled with anhydrous sodium sulphate as a drying medium. In total, the fractionation procedure extracted o

Druh

O - Ostatní výsledky

CEP obor

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OECD FORD obor

10403 - Physical chemistry

Projekt

<a href="/cs/project/GJ20-28208Y" target="_blank" >GJ20-28208Y: Studium vlivu aplikace biouhlu na transformaci půdní organické hmoty – od multidisciplinární metodiky po interpretaci na molekulární úrovni</a><br>

Návaznosti

P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Rok uplatnění

2021

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů