Effects of anodizing conditions and the addition of Al2O3/PTFE particles on the microstructure and the mechanical properties of porous anodic coatings on the AA1050 aluminium alloy

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216305%3A26620%2F20%3APU135794" target="_blank" >RIV/00216305:26620/20:PU135794 - isvavai.cz</a>

Výsledek na webu

<a href="https://authors.elsevier.com/a/1ae-ncXa%7EwD7L" target="_blank" >https://authors.elsevier.com/a/1ae-ncXa%7EwD7L</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1016/j.apsusc.2020.145780" target="_blank" >10.1016/j.apsusc.2020.145780</a>

Jazyk výsledku

angličtina

Název v původním jazyce

Effects of anodizing conditions and the addition of Al2O3/PTFE particles on the microstructure and the mechanical properties of porous anodic coatings on the AA1050 aluminium alloy

Popis výsledku v původním jazyce

In the present study, porous anodic aluminium oxide (AAO) coatings with and without particles of Al2O3 (aluminium oxide) and polytetrafluorethylene (PTFE) were produced on AA1050 aluminium alloy via galvanostatic anodizing in acidic electrolyte. The effects of anodizing conditions (i.e. temperature, current density and composition of electrolyte) on the morphology, thickness, and microhardness were studied via scanning electron microscopy (SEM) equipped with energy dispersive X-ray spectroscopy (EDX) and Vickers hardness tester. The results showed that the decrease of electrolyte temperature from 24 to 10 °C and the addition of 20 g/L oxalic acid to 15% H2SO4 electrolyte led to the formation of thicker (34 µm) and harder porous AAO coating with hillocks. Furthermore, the decrease of applied current density from 3 to 1 A/dm2 resulted in the formation of thinner coating (10 µm) without hillocks. The intermetallic phases based on Al-Fe and Al-Fe-Si compounds present in AA1050 alloy were not preferably dissoluted during the anodizing process at 10 °C of electrolyte. The tribological properties of the anodic coatings were investigated by the dry friction test. The results showed that the addition of Al2O3 and PTFE particles to sulfuric-oxalic acid electrolyte resulted in hard anodic composite coatings with enhanced wear resistance.

Název v anglickém jazyce

Effects of anodizing conditions and the addition of Al2O3/PTFE particles on the microstructure and the mechanical properties of porous anodic coatings on the AA1050 aluminium alloy

Popis výsledku anglicky

In the present study, porous anodic aluminium oxide (AAO) coatings with and without particles of Al2O3 (aluminium oxide) and polytetrafluorethylene (PTFE) were produced on AA1050 aluminium alloy via galvanostatic anodizing in acidic electrolyte. The effects of anodizing conditions (i.e. temperature, current density and composition of electrolyte) on the morphology, thickness, and microhardness were studied via scanning electron microscopy (SEM) equipped with energy dispersive X-ray spectroscopy (EDX) and Vickers hardness tester. The results showed that the decrease of electrolyte temperature from 24 to 10 °C and the addition of 20 g/L oxalic acid to 15% H2SO4 electrolyte led to the formation of thicker (34 µm) and harder porous AAO coating with hillocks. Furthermore, the decrease of applied current density from 3 to 1 A/dm2 resulted in the formation of thinner coating (10 µm) without hillocks. The intermetallic phases based on Al-Fe and Al-Fe-Si compounds present in AA1050 alloy were not preferably dissoluted during the anodizing process at 10 °C of electrolyte. The tribological properties of the anodic coatings were investigated by the dry friction test. The results showed that the addition of Al2O3 and PTFE particles to sulfuric-oxalic acid electrolyte resulted in hard anodic composite coatings with enhanced wear resistance.

Druh

J_imp - Článek v periodiku v databázi Web of Science

CEP obor

—

OECD FORD obor

20506 - Coating and films

Projekt

Výsledek vznikl pri realizaci vícero projektů. Více informací v záložce Projekty.

Návaznosti

P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>S - Specificky vyzkum na vysokych skolach

Rok uplatnění

2020

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Název periodika

Applied Surface Science

ISSN

0169-4332

e-ISSN

1873-5584

Svazek periodika

513

Číslo periodika v rámci svazku

145780

Stát vydavatele periodika

NL - Nizozemsko

Počet stran výsledku

10

Strana od-do

1-10

Kód UT WoS článku

000523184600034

EID výsledku v databázi Scopus

2-s2.0-85080044568