Kinetics of Static Recrystallization in the Coarse-grained Fe–40 At.%Al–Zr–B Alloy

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F46747885%3A24210%2F17%3A00004123" target="_blank" >RIV/46747885:24210/17:00004123 - isvavai.cz</a>

Nalezeny alternativní kódy

RIV/61989100:27360/17:10238539 RIV/68378271:_____/17:00502068

Výsledek na webu

<a href="http://www.sciencedirect.com/science/article/pii/S1644966517300341" target="_blank" >http://www.sciencedirect.com/science/article/pii/S1644966517300341</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1016/j.acme.2017.03.004" target="_blank" >10.1016/j.acme.2017.03.004</a>

Jazyk výsledku

angličtina

Název v původním jazyce

Kinetics of Static Recrystallization in the Coarse-grained Fe–40 At.%Al–Zr–B Alloy

Popis výsledku v původním jazyce

The aim of works was to describe mathematically the kinetics of static recrystallization of the alloy type Fe–40 at.%Al–Zr–B (with 24.6 Al–0.01 B–0.18 Zr–0.01 C in wt.%) with the coarse-grained structure. The microstructure of the laboratory castings made of this extremely brittle alloy was homogenized by hot rolling of the material in the protective capsules and by the long-term annealing at 1200 °C. An initial microstructure with average grain size 0.77 &plusmn; 0.27 mm was obtained. Based on the isothermal plastic deformation tests and EBSD analysis, the static recrystallization kinetics of the prepared coarse-grained B2 iron aluminide after strain 0.20 was mathematically described. Recrystallized fraction depends on deformation/annealing temperature (900–1100 °C) as well as on annealing time. The activation energy of static recrystallization was calculated as 255 kJ mol-1. Competition between dynamic recovery and static recrystallization was proved after strain 0.35 and annealing temperature 1100 °C. Static recrystallization starts relatively easily in the studied alloy, but a very long-term annealing is quite necessary for the complete course of recrystallization. The mean size of recrystallized grains falls with the decreasing annealing temperature (0.47 &plusmn; 0.15 mm for temperature 1100 °C, and 0.22 &plusmn; 0.04 mm for 900 °C). Even at a temperature of 1200 °C the annealing after deformation should last approx. 1 min for obtaining the fully recrystallized microstructure. That is why the standard hot forming technologies should be combined by an interpass annealing in order to refine sufficiently the coarse grains.

Název v anglickém jazyce

Kinetics of Static Recrystallization in the Coarse-grained Fe–40 At.%Al–Zr–B Alloy

Popis výsledku anglicky

The aim of works was to describe mathematically the kinetics of static recrystallization of the alloy type Fe–40 at.%Al–Zr–B (with 24.6 Al–0.01 B–0.18 Zr–0.01 C in wt.%) with the coarse-grained structure. The microstructure of the laboratory castings made of this extremely brittle alloy was homogenized by hot rolling of the material in the protective capsules and by the long-term annealing at 1200 °C. An initial microstructure with average grain size 0.77 &plusmn; 0.27 mm was obtained. Based on the isothermal plastic deformation tests and EBSD analysis, the static recrystallization kinetics of the prepared coarse-grained B2 iron aluminide after strain 0.20 was mathematically described. Recrystallized fraction depends on deformation/annealing temperature (900–1100 °C) as well as on annealing time. The activation energy of static recrystallization was calculated as 255 kJ mol-1. Competition between dynamic recovery and static recrystallization was proved after strain 0.35 and annealing temperature 1100 °C. Static recrystallization starts relatively easily in the studied alloy, but a very long-term annealing is quite necessary for the complete course of recrystallization. The mean size of recrystallized grains falls with the decreasing annealing temperature (0.47 &plusmn; 0.15 mm for temperature 1100 °C, and 0.22 &plusmn; 0.04 mm for 900 °C). Even at a temperature of 1200 °C the annealing after deformation should last approx. 1 min for obtaining the fully recrystallized microstructure. That is why the standard hot forming technologies should be combined by an interpass annealing in order to refine sufficiently the coarse grains.

Druh

J_imp - Článek v periodiku v databázi Web of Science

CEP obor

—

OECD FORD obor

20501 - Materials engineering

Projekt

Výsledek vznikl pri realizaci vícero projektů. Více informací v záložce Projekty.

Návaznosti

P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Rok uplatnění

2017

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Název periodika

Archives of Civil and Mechanical Engineering

ISSN

1644-9665

e-ISSN

—

Svazek periodika

17

Číslo periodika v rámci svazku

4

Stát vydavatele periodika

PL - Polská republika

Počet stran výsledku

11

Strana od-do

816-826

Kód UT WoS článku

000416528900009

EID výsledku v databázi Scopus

2-s2.0-85017691132