Antimony nanomaterials modified screen-printed electrodes for the voltammetric determination of metal ions
Identifikátory výsledku
Kód výsledku v IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22310%2F22%3A43924177" target="_blank" >RIV/60461373:22310/22:43924177 - isvavai.cz</a>
Výsledek na webu
<a href="https://www.sciencedirect.com/science/article/pii/S0013468622008490" target="_blank" >https://www.sciencedirect.com/science/article/pii/S0013468622008490</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1016/j.electacta.2022.140690" target="_blank" >10.1016/j.electacta.2022.140690</a>
Alternativní jazyky
Jazyk výsledku
angličtina
Název v původním jazyce
Antimony nanomaterials modified screen-printed electrodes for the voltammetric determination of metal ions
Popis výsledku v původním jazyce
Exfoliated β-Sb or two dimensional (2D) antimonene-based modified screen-printed electrode (2D Sb-SPCE), prepared by drop-casting of an exfoliated layered β-antimony (2D Sb) suspension, was used for the simultaneous determination of Pb(II) and Cd(II) by differential pulse anodic stripping voltammetry (DPASV). 2D Sb-SPCE was characterized by microscopic and analytical techniques, and compared not only to bare SPCE but also to layered antimony chalcogenides based-sensors. Both Sb2S3 and Sb2Se3 have an isomorphous tubular one-dimensional (1D) crystal structure, whereas Sb2Te3 and monoelement β-Sb have a 2D layered structure. Under optimized conditions, 2D Sb-SPCE displays an excellent analytical performance with detection limits of 0.3 and 2.7 μg L−1 for Pb(II) and Cd(II), respectively, and a linear response from 1.1 to 128.3 µg L−1 for Pb(II) and from 9.1 to 132.7 µg L−1 for Cd(II). Moreover, 2D Sb-SPCE was successfully applied for the DPASV determination of Pb(II) and Cd(II) in tap water, achieving statistically comparable results to those provided by ICP-MS measurements. © 2022
Název v anglickém jazyce
Antimony nanomaterials modified screen-printed electrodes for the voltammetric determination of metal ions
Popis výsledku anglicky
Exfoliated β-Sb or two dimensional (2D) antimonene-based modified screen-printed electrode (2D Sb-SPCE), prepared by drop-casting of an exfoliated layered β-antimony (2D Sb) suspension, was used for the simultaneous determination of Pb(II) and Cd(II) by differential pulse anodic stripping voltammetry (DPASV). 2D Sb-SPCE was characterized by microscopic and analytical techniques, and compared not only to bare SPCE but also to layered antimony chalcogenides based-sensors. Both Sb2S3 and Sb2Se3 have an isomorphous tubular one-dimensional (1D) crystal structure, whereas Sb2Te3 and monoelement β-Sb have a 2D layered structure. Under optimized conditions, 2D Sb-SPCE displays an excellent analytical performance with detection limits of 0.3 and 2.7 μg L−1 for Pb(II) and Cd(II), respectively, and a linear response from 1.1 to 128.3 µg L−1 for Pb(II) and from 9.1 to 132.7 µg L−1 for Cd(II). Moreover, 2D Sb-SPCE was successfully applied for the DPASV determination of Pb(II) and Cd(II) in tap water, achieving statistically comparable results to those provided by ICP-MS measurements. © 2022
Klasifikace
Druh
J<sub>imp</sub> - Článek v periodiku v databázi Web of Science
CEP obor
—
OECD FORD obor
10405 - Electrochemistry (dry cells, batteries, fuel cells, corrosion metals, electrolysis)
Návaznosti výsledku
Projekt
<a href="/cs/project/GX19-26910X" target="_blank" >GX19-26910X: Chemie ve dvou dimenzích - za hranice grafenu</a><br>
Návaznosti
P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)
Ostatní
Rok uplatnění
2022
Kód důvěrnosti údajů
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Údaje specifické pro druh výsledku
Název periodika
Electrochimica Acta
ISSN
0013-4686
e-ISSN
1873-3859
Svazek periodika
425
Číslo periodika v rámci svazku
1 September 2022
Stát vydavatele periodika
GB - Spojené království Velké Británie a Severního Irska
Počet stran výsledku
11
Strana od-do
nestrankovano
Kód UT WoS článku
000819372000001
EID výsledku v databázi Scopus
2-s2.0-85132780843