Analysis of mycotoxins in barley using ultra high liquid chromatography high resolution mass spectrometry: Comparison of efficiency and efficacy of different extraction procedures
Identifikátory výsledku
Kód výsledku v IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22330%2F12%3A43894809" target="_blank" >RIV/60461373:22330/12:43894809 - isvavai.cz</a>
Výsledek na webu
<a href="http://dx.doi.org/10.1016/j.talanta.2012.07.010" target="_blank" >http://dx.doi.org/10.1016/j.talanta.2012.07.010</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1016/j.talanta.2012.07.010" target="_blank" >10.1016/j.talanta.2012.07.010</a>
Alternativní jazyky
Jazyk výsledku
angličtina
Název v původním jazyce
Analysis of mycotoxins in barley using ultra high liquid chromatography high resolution mass spectrometry: Comparison of efficiency and efficacy of different extraction procedures
Popis výsledku v původním jazyce
The effectiveness of four extraction methods (modified QuEChERS, matrix solid-phase dispersion (MSPD), solid-liquid extraction (SLE) and solid-phase extraction (SPE clean-up) were evaluated for simultaneous determination of 32 mycotoxins produced by thegenus Fusarium, Claviceps, Aspergillus, Penicillium and Alternaria in barely by ultra high pressure liquid chromatography coupled to ultra-high resolution mass spectrometry (UHPLC-Orbitrap MS). The efficiency and efficacy of extraction methods were evaluated and compared in number of extracted mycotoxins and obtained recoveries. From the one point of view, QuEChERS procedure was fast and easy, as well as it was able to successfully extract all selected mycotoxins. On the other hand, SLE method, MSPD andSPE clean-up method did not extracted equally all selected mycotoxins and recoveries were not suitable enough. Thereby, method employing QuEChERS extraction connected with UHPLC-Orbitrap MS was developer to quantify 32 mycotoxins in bare
Název v anglickém jazyce
Analysis of mycotoxins in barley using ultra high liquid chromatography high resolution mass spectrometry: Comparison of efficiency and efficacy of different extraction procedures
Popis výsledku anglicky
The effectiveness of four extraction methods (modified QuEChERS, matrix solid-phase dispersion (MSPD), solid-liquid extraction (SLE) and solid-phase extraction (SPE clean-up) were evaluated for simultaneous determination of 32 mycotoxins produced by thegenus Fusarium, Claviceps, Aspergillus, Penicillium and Alternaria in barely by ultra high pressure liquid chromatography coupled to ultra-high resolution mass spectrometry (UHPLC-Orbitrap MS). The efficiency and efficacy of extraction methods were evaluated and compared in number of extracted mycotoxins and obtained recoveries. From the one point of view, QuEChERS procedure was fast and easy, as well as it was able to successfully extract all selected mycotoxins. On the other hand, SLE method, MSPD andSPE clean-up method did not extracted equally all selected mycotoxins and recoveries were not suitable enough. Thereby, method employing QuEChERS extraction connected with UHPLC-Orbitrap MS was developer to quantify 32 mycotoxins in bare
Klasifikace
Druh
J<sub>x</sub> - Nezařazeno - Článek v odborném periodiku (Jimp, Jsc a Jost)
CEP obor
GM - Potravinářství
OECD FORD obor
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Návaznosti výsledku
Projekt
Výsledek vznikl pri realizaci vícero projektů. Více informací v záložce Projekty.
Návaznosti
P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)
Ostatní
Rok uplatnění
2012
Kód důvěrnosti údajů
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Údaje specifické pro druh výsledku
Název periodika
Talanta
ISSN
0039-9140
e-ISSN
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Svazek periodika
2012
Číslo periodika v rámci svazku
99
Stát vydavatele periodika
NL - Nizozemsko
Počet stran výsledku
8
Strana od-do
712-719
Kód UT WoS článku
000309785300102
EID výsledku v databázi Scopus
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