Obtaining of silver nanopowders by the thermal decomposition of fatty silver salts with various chain length
Identifikátory výsledku
Kód výsledku v IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61389013%3A_____%2F19%3A00503877" target="_blank" >RIV/61389013:_____/19:00503877 - isvavai.cz</a>
Výsledek na webu
<a href="https://iopscience.iop.org/article/10.1088/2053-1591/ab086b" target="_blank" >https://iopscience.iop.org/article/10.1088/2053-1591/ab086b</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1088/2053-1591/ab086b" target="_blank" >10.1088/2053-1591/ab086b</a>
Alternativní jazyky
Jazyk výsledku
angličtina
Název v původním jazyce
Obtaining of silver nanopowders by the thermal decomposition of fatty silver salts with various chain length
Popis výsledku v původním jazyce
In the present study authors describe results of research on silver structures obtained by the thermal decomposition process of organic precursors. Silver nanoparticles obtained during process had different size and structure morphology. Length of precursors carbon chain impact on silver nanopowders quality have been proved. Obtaining particles authors paid attention on silver phase forming mechanism during silver grains aggregations, and also on structural deformation process. Temperatures of precursor decompositions were define precisely with consider of carbon atoms quantity in their carboxylate chains. Activation energy of the test specimens was analyzed with use of thermogravimetric method. The correctness of whole process—from precursors synthesis to their thermal decomposition, were investigated by NMR spectra. Examples of correct silver structures and structural deformations were characterized by SEM imaging. Classification of obtained structures allowed to determine optimal conditions for thermal decomposition process for silver nanopowders production.
Název v anglickém jazyce
Obtaining of silver nanopowders by the thermal decomposition of fatty silver salts with various chain length
Popis výsledku anglicky
In the present study authors describe results of research on silver structures obtained by the thermal decomposition process of organic precursors. Silver nanoparticles obtained during process had different size and structure morphology. Length of precursors carbon chain impact on silver nanopowders quality have been proved. Obtaining particles authors paid attention on silver phase forming mechanism during silver grains aggregations, and also on structural deformation process. Temperatures of precursor decompositions were define precisely with consider of carbon atoms quantity in their carboxylate chains. Activation energy of the test specimens was analyzed with use of thermogravimetric method. The correctness of whole process—from precursors synthesis to their thermal decomposition, were investigated by NMR spectra. Examples of correct silver structures and structural deformations were characterized by SEM imaging. Classification of obtained structures allowed to determine optimal conditions for thermal decomposition process for silver nanopowders production.
Klasifikace
Druh
J<sub>imp</sub> - Článek v periodiku v databázi Web of Science
CEP obor
—
OECD FORD obor
10404 - Polymer science
Návaznosti výsledku
Projekt
—
Návaznosti
I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace
Ostatní
Rok uplatnění
2019
Kód důvěrnosti údajů
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Údaje specifické pro druh výsledku
Název periodika
Materials Research Express
ISSN
2053-1591
e-ISSN
—
Svazek periodika
6
Číslo periodika v rámci svazku
6
Stát vydavatele periodika
GB - Spojené království Velké Británie a Severního Irska
Počet stran výsledku
9
Strana od-do
1-9
Kód UT WoS článku
000462896700002
EID výsledku v databázi Scopus
2-s2.0-85064483989