On reactive suspension plasma spraying of calcium titanate

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61389021%3A_____%2F16%3A00459826" target="_blank" >RIV/61389021:_____/16:00459826 - isvavai.cz</a>

Nalezeny alternativní kódy

RIV/68407700:21230/16:00235574

Výsledek na webu

<a href="http://dx.doi.org/10.1016/j.ceramint.2015.11.159" target="_blank" >http://dx.doi.org/10.1016/j.ceramint.2015.11.159</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1016/j.ceramint.2015.11.159" target="_blank" >10.1016/j.ceramint.2015.11.159</a>

Jazyk výsledku

angličtina

Název v původním jazyce

On reactive suspension plasma spraying of calcium titanate

Popis výsledku v původním jazyce

This study shows possibility of preparation of calcium titanate powder and coatings by reactive suspension plasma spraying. Suspension of mixture of calcium carbonate (CaCO3) and titanium dioxide (TiO2) powders in ethanol was fed into hybrid plasma torch with a DC-arc stabilized by a water–argon mixture (WSP-H 500). Various feeding distances and angles were used in order to optimize suspension feeding conditions. In the next step, the coatings were deposited on stainless steel substrates and the effect of substrate temperature on microstructure and chemical and phase composition of the coatings was studied. Captured in-flight particles and deposits were analysed by X-ray diffraction (XRD) and scanning electron microscopy SEM equipped with EDX detector. Obtained results confirm that chemical reaction of CaCO3 and TiO2 forming CaTiO3 perovskite takes place during the interaction of suspension with plasma jet. The conditions of rapid cooling during spraying process result in the presence of metastable CaTiO3 high-temperature tetragonal and cubic phases. Increase in the substrate temperature increases the content of the calcium titanate in the deposit and the coatings microstructure becomes more compact. Obtained results show that WSP-H technology may be used for deposition of the CaTiO3 powders and coatings by reactive plasma spraying.

Název v anglickém jazyce

On reactive suspension plasma spraying of calcium titanate

Popis výsledku anglicky

This study shows possibility of preparation of calcium titanate powder and coatings by reactive suspension plasma spraying. Suspension of mixture of calcium carbonate (CaCO3) and titanium dioxide (TiO2) powders in ethanol was fed into hybrid plasma torch with a DC-arc stabilized by a water–argon mixture (WSP-H 500). Various feeding distances and angles were used in order to optimize suspension feeding conditions. In the next step, the coatings were deposited on stainless steel substrates and the effect of substrate temperature on microstructure and chemical and phase composition of the coatings was studied. Captured in-flight particles and deposits were analysed by X-ray diffraction (XRD) and scanning electron microscopy SEM equipped with EDX detector. Obtained results confirm that chemical reaction of CaCO3 and TiO2 forming CaTiO3 perovskite takes place during the interaction of suspension with plasma jet. The conditions of rapid cooling during spraying process result in the presence of metastable CaTiO3 high-temperature tetragonal and cubic phases. Increase in the substrate temperature increases the content of the calcium titanate in the deposit and the coatings microstructure becomes more compact. Obtained results show that WSP-H technology may be used for deposition of the CaTiO3 powders and coatings by reactive plasma spraying.

Druh

J_x - Nezařazeno - Článek v odborném periodiku (Jimp, Jsc a Jost)

CEP obor

JH - Keramika, žáruvzdorné materiály a skla

OECD FORD obor

—

Projekt

<a href="/cs/project/GA15-12145S" target="_blank" >GA15-12145S: Fyzikální aspekty depozice plazmových nástřiků z kapalné fáze</a><br>

Návaznosti

I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Rok uplatnění

2016

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Název periodika

Ceramics International

ISSN

0272-8842

e-ISSN

—

Svazek periodika

42

Číslo periodika v rámci svazku

3

Stát vydavatele periodika

GB - Spojené království Velké Británie a Severního Irska

Počet stran výsledku

9

Strana od-do

4607-4615

Kód UT WoS článku

000369190900108

EID výsledku v databázi Scopus

2-s2.0-84949641184