Determination of Acrylamide and Acrolein in Smoke from Tobacco and E-Cigarettes

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61989592%3A15310%2F14%3A33151478" target="_blank" >RIV/61989592:15310/14:33151478 - isvavai.cz</a>

Výsledek na webu

<a href="http://download.springer.com/static/pdf/506/art%253A10.1007%252Fs10337-014-2729-2.pdf?auth66=1422270803_3c407b4d393241eb4dea7842e189cef1&ext=.pdf" target="_blank" >http://download.springer.com/static/pdf/506/art%253A10.1007%252Fs10337-014-2729-2.pdf?auth66=1422270803_3c407b4d393241eb4dea7842e189cef1&ext=.pdf</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1007/s10337-014-2729-2" target="_blank" >10.1007/s10337-014-2729-2</a>

Jazyk výsledku

angličtina

Název v původním jazyce

Determination of Acrylamide and Acrolein in Smoke from Tobacco and E-Cigarettes

Popis výsledku v původním jazyce

Acrylamide and acrolein are two short-chained hazardous compounds with neurotoxic, carcinogenic, and mutagenic effects. The aim of this paper is to describe a fast and simple procedure for simultaneous determination of both acrylamide and acrolein understandard conditions, suggest a suitable calibration protocol for custom analysis, and demonstrate its applicability to the analysis of gaseous products from, e.g., cigarettes, cigars, or electronic cigarettes. A gas chromatography-mass spectrometry (GC-MS) method was developed to quantify acrylamide and acrolein in smoke vapor from electronic cigarettes, tobacco cigarettes, and cigars. Nonionic and highly polar molecules with a low boiling point and molecular mass need a suitable derivatization method to achieve appropriate retention and selectivity on commonly used relatively nonpolar stationary phases and to enhance the molecular mass for easy MS detection. The derivatization of acrylamide and acrolein was carried out by a bromination

Název v anglickém jazyce

Determination of Acrylamide and Acrolein in Smoke from Tobacco and E-Cigarettes

Popis výsledku anglicky

Acrylamide and acrolein are two short-chained hazardous compounds with neurotoxic, carcinogenic, and mutagenic effects. The aim of this paper is to describe a fast and simple procedure for simultaneous determination of both acrylamide and acrolein understandard conditions, suggest a suitable calibration protocol for custom analysis, and demonstrate its applicability to the analysis of gaseous products from, e.g., cigarettes, cigars, or electronic cigarettes. A gas chromatography-mass spectrometry (GC-MS) method was developed to quantify acrylamide and acrolein in smoke vapor from electronic cigarettes, tobacco cigarettes, and cigars. Nonionic and highly polar molecules with a low boiling point and molecular mass need a suitable derivatization method to achieve appropriate retention and selectivity on commonly used relatively nonpolar stationary phases and to enhance the molecular mass for easy MS detection. The derivatization of acrylamide and acrolein was carried out by a bromination

Druh

J_x - Nezařazeno - Článek v odborném periodiku (Jimp, Jsc a Jost)

CEP obor

CB - Analytická chemie, separace

OECD FORD obor

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Projekt

Výsledek vznikl pri realizaci vícero projektů. Více informací v záložce Projekty.

Návaznosti

P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>S - Specificky vyzkum na vysokych skolach

Rok uplatnění

2014

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Název periodika

Chromatographia

ISSN

0009-5893

e-ISSN

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Svazek periodika

77

Číslo periodika v rámci svazku

17-18

Stát vydavatele periodika

DE - Spolková republika Německo

Počet stran výsledku

7

Strana od-do

1145-1151

Kód UT WoS článku

000341659000005

EID výsledku v databázi Scopus

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