Using Mössbauer Spectroscopy to Evaluate the Influence of Heat Treatment on the Surface Characteristics of Additive Manufactured 316L Stainless Steel

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61989592%3A15310%2F24%3A73625520" target="_blank" >RIV/61989592:15310/24:73625520 - isvavai.cz</a>

Výsledek na webu

<a href="https://www.mdpi.com/1996-1944/17/14/3494" target="_blank" >https://www.mdpi.com/1996-1944/17/14/3494</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.3390/ma17143494" target="_blank" >10.3390/ma17143494</a>

Jazyk výsledku

angličtina

Název v původním jazyce

Using Mössbauer Spectroscopy to Evaluate the Influence of Heat Treatment on the Surface Characteristics of Additive Manufactured 316L Stainless Steel

Popis výsledku v původním jazyce

The oxidation behaviour of iron-based 316L stainless steel was investigated in the temperature range of 700 to 1000 °C. The test specimens in the shape of plates were produced by selective laser melting. After fabrication, the samples were sandblasted and then annealed in air for different periods of time (0.5, 2, 8, 32 h). Under the influence of temperature and time, stainless steels tend to form an oxide layer. Scanning electron microscopy, energy dispersive analysis, and X-ray diffraction were employed to analyse the composition of this layer. Notably, a thin oxide layer primarily composed of (Fe-Cr) formed on the surface due to temperature effects. In addition, with increasing temperature (up to 1000 °C), the oxide of the main alloying elements, specifically Mn2(Fe-Cr)O4, appeared alongside the Fe-Cr oxide. Furthermore, the samples were subjected to conversion X-ray (CXMS) and conversion electron (CEMS) Mössbauer spectroscopy. CXMS revealed a singlet with a decreasing Mössbauer effect based on the surface metal oxide thickness. CEMS revealed the presence of Fe3+ in the surface layer (0.3 µm). Moreover, an interesting phenomenon occurred at higher temperature levels due to the inhomogeneously thick surface metal oxide layer and the tangential direction of the Mössbauer radiation towards the electron detector.

Název v anglickém jazyce

Using Mössbauer Spectroscopy to Evaluate the Influence of Heat Treatment on the Surface Characteristics of Additive Manufactured 316L Stainless Steel

Popis výsledku anglicky

The oxidation behaviour of iron-based 316L stainless steel was investigated in the temperature range of 700 to 1000 °C. The test specimens in the shape of plates were produced by selective laser melting. After fabrication, the samples were sandblasted and then annealed in air for different periods of time (0.5, 2, 8, 32 h). Under the influence of temperature and time, stainless steels tend to form an oxide layer. Scanning electron microscopy, energy dispersive analysis, and X-ray diffraction were employed to analyse the composition of this layer. Notably, a thin oxide layer primarily composed of (Fe-Cr) formed on the surface due to temperature effects. In addition, with increasing temperature (up to 1000 °C), the oxide of the main alloying elements, specifically Mn2(Fe-Cr)O4, appeared alongside the Fe-Cr oxide. Furthermore, the samples were subjected to conversion X-ray (CXMS) and conversion electron (CEMS) Mössbauer spectroscopy. CXMS revealed a singlet with a decreasing Mössbauer effect based on the surface metal oxide thickness. CEMS revealed the presence of Fe3+ in the surface layer (0.3 µm). Moreover, an interesting phenomenon occurred at higher temperature levels due to the inhomogeneously thick surface metal oxide layer and the tangential direction of the Mössbauer radiation towards the electron detector.

Druh

J_imp - Článek v periodiku v databázi Web of Science

CEP obor

—

OECD FORD obor

20501 - Materials engineering

Projekt

<a href="/cs/project/EF17_049%2F0008408" target="_blank" >EF17_049/0008408: Hydrodynamický design čerpadel</a><br>

Návaznosti

P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>S - Specificky vyzkum na vysokych skolach

Rok uplatnění

2024

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Název periodika

Materials

ISSN

1996-1944

e-ISSN

—

Svazek periodika

17

Číslo periodika v rámci svazku

14

Stát vydavatele periodika

CH - Švýcarská konfederace

Počet stran výsledku

16

Strana od-do

"3494-1"-"3494-16"

Kód UT WoS článku

001277417800001

EID výsledku v databázi Scopus

2-s2.0-85199794638