Synthesis, characterization and thermal studies of a nanosized 1D L-Arginine/Copper(II) coordination polymer by sonochemical method: a new precursor for preparation of copper(II) oxide nanoparticles

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378271%3A_____%2F20%3A00533714" target="_blank" >RIV/68378271:_____/20:00533714 - isvavai.cz</a>

Výsledek na webu

<a href="https://doi.org/10.1007/s10904-020-01442-8" target="_blank" >https://doi.org/10.1007/s10904-020-01442-8</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1007/s10904-020-01442-8" target="_blank" >10.1007/s10904-020-01442-8</a>

Jazyk výsledku

angličtina

Název v původním jazyce

Synthesis, characterization and thermal studies of a nanosized 1D L-Arginine/Copper(II) coordination polymer by sonochemical method: a new precursor for preparation of copper(II) oxide nanoparticles

Popis výsledku v původním jazyce

In the present work, 1D-copper(II) coordination polymer, {[Cu(μ-l-Arg)2(H2O)]SO4}n (1), (l-Arg: l-Arginine), was synthesized and identified by elemental analysis, FT-IR spectroscopy, molar conductivity, thermal gravimetric analysis (TGA), differential thermal analysis (DTA) and single-crystal X-ray diffraction. The compound 1 was also prepared by a sonochemical process in the form of nanoparticles. The particle size and morphology of the synthesized nanoparticles were investigated by powder X-ray diffraction (PXRD) and field emission scanning electron microscopy (FE-SEM). Finally, CuO nanoparti cles were produced by thermal decomposition of the sonochemically prepared nanoparticles of 1, and characterized by FT-IR, XRD, FE-SEM and EDS.

Název v anglickém jazyce

Synthesis, characterization and thermal studies of a nanosized 1D L-Arginine/Copper(II) coordination polymer by sonochemical method: a new precursor for preparation of copper(II) oxide nanoparticles

Popis výsledku anglicky

In the present work, 1D-copper(II) coordination polymer, {[Cu(μ-l-Arg)2(H2O)]SO4}n (1), (l-Arg: l-Arginine), was synthesized and identified by elemental analysis, FT-IR spectroscopy, molar conductivity, thermal gravimetric analysis (TGA), differential thermal analysis (DTA) and single-crystal X-ray diffraction. The compound 1 was also prepared by a sonochemical process in the form of nanoparticles. The particle size and morphology of the synthesized nanoparticles were investigated by powder X-ray diffraction (PXRD) and field emission scanning electron microscopy (FE-SEM). Finally, CuO nanoparti cles were produced by thermal decomposition of the sonochemically prepared nanoparticles of 1, and characterized by FT-IR, XRD, FE-SEM and EDS.

Druh

J_imp - Článek v periodiku v databázi Web of Science

CEP obor

—

OECD FORD obor

10302 - Condensed matter physics (including formerly solid state physics, supercond.)

Projekt

Výsledek vznikl pri realizaci vícero projektů. Více informací v záložce Projekty.

Návaznosti

I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Rok uplatnění

2020

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Název periodika

Journal of Inorganic and Organometallic Polymers and Materials

ISSN

1574-1443

e-ISSN

—

Svazek periodika

30

Číslo periodika v rámci svazku

8

Stát vydavatele periodika

US - Spojené státy americké

Počet stran výsledku

8

Strana od-do

2907-2915

Kód UT WoS článku

000547945500009

EID výsledku v databázi Scopus

2-s2.0-85077624373