Reaction monitoring of cementing materials through multivariate techniques applied to time-resolved synchrotron X-Ray diffraction data
Identifikátory výsledku
Kód výsledku v IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378297%3A_____%2F15%3A00452611" target="_blank" >RIV/68378297:_____/15:00452611 - isvavai.cz</a>
Výsledek na webu
<a href="http://www.aidic.it/cet/15/43/150.pdf" target="_blank" >http://www.aidic.it/cet/15/43/150.pdf</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.3303/CET1543150" target="_blank" >10.3303/CET1543150</a>
Alternativní jazyky
Jazyk výsledku
angličtina
Název v původním jazyce
Reaction monitoring of cementing materials through multivariate techniques applied to time-resolved synchrotron X-Ray diffraction data
Popis výsledku v původním jazyce
In this work, the setting reaction of magnesium potassium phosphate ceramic (MKPC) from magnesia (MgO) and potassium di-hydrogen phosphate was investigated by means of in-situ synchrotron X-ray powder diffraction (XRPD). The experimental data were analyzed through multivariate statistical techniques that enabled a real time and reliable understanding of the phenomena occurring in the process. Here, a method combining Multivariate Curve Resolution-Alternating Least Squares (MCR-ALS) with Evolving FactorAnalysis (EFA) was proposed. Comparison with the conventional methods showed that the compounds involved in the process can be correctly distinguished and the main reaction steps, such as reactants consumption, occurrence of intermediate amorphous phaseand MKPC formation can be clearly identified.
Název v anglickém jazyce
Reaction monitoring of cementing materials through multivariate techniques applied to time-resolved synchrotron X-Ray diffraction data
Popis výsledku anglicky
In this work, the setting reaction of magnesium potassium phosphate ceramic (MKPC) from magnesia (MgO) and potassium di-hydrogen phosphate was investigated by means of in-situ synchrotron X-ray powder diffraction (XRPD). The experimental data were analyzed through multivariate statistical techniques that enabled a real time and reliable understanding of the phenomena occurring in the process. Here, a method combining Multivariate Curve Resolution-Alternating Least Squares (MCR-ALS) with Evolving FactorAnalysis (EFA) was proposed. Comparison with the conventional methods showed that the compounds involved in the process can be correctly distinguished and the main reaction steps, such as reactants consumption, occurrence of intermediate amorphous phaseand MKPC formation can be clearly identified.
Klasifikace
Druh
J<sub>x</sub> - Nezařazeno - Článek v odborném periodiku (Jimp, Jsc a Jost)
CEP obor
AN - Psychologie
OECD FORD obor
—
Návaznosti výsledku
Projekt
<a href="/cs/project/LO1219" target="_blank" >LO1219: Udržitelný pokročilý rozvoj CET</a><br>
Návaznosti
P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)
Ostatní
Rok uplatnění
2015
Kód důvěrnosti údajů
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Údaje specifické pro druh výsledku
Název periodika
Chemical Engineering Transactions
ISSN
2283-9216
e-ISSN
—
Svazek periodika
43
Číslo periodika v rámci svazku
May
Stát vydavatele periodika
IT - Italská republika
Počet stran výsledku
6
Strana od-do
895-900
Kód UT WoS článku
000365994200150
EID výsledku v databázi Scopus
2-s2.0-84946080121