In-situ measurement of particle size distribution in an agitated vessel

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68407700%3A21220%2F17%3A00324241" target="_blank" >RIV/68407700:21220/17:00324241 - isvavai.cz</a>

Nalezeny alternativní kódy

RIV/67985874:_____/17:00482416

Výsledek na webu

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DOI - Digital Object Identifier

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Jazyk výsledku

angličtina

Název v původním jazyce

In-situ measurement of particle size distribution in an agitated vessel

Popis výsledku v původním jazyce

Agitation of solid-liquid suspension or two immiscible liquids is a frequent operation in chemical and metallurgical industries (suspension/emulsion polymerization, catalytic chemical reaction, hydrometallurgical solvent extraction). The product quality, yield and economy of the processes are significantly affected by a mixing process. Prediction of mean particle/drop size and particle/drop size distribution (PSD) during the agitation is fundamental for emulsification, suspension polymerization, solid particle dispersion or crystallization. The aim of this contribution is to propose a simple method of in-situ measurement of particle size distribution. The particle size measurement is based on an image analysis performed on raw image records. Evaluation method based on the best focused particles with sharp detected boundaries enhanced by the analysis of particle circularity was developed. Precise spherical mono-disperse steel and plastic particles were used to verify accuracy of evaluation method. The method has been proposed for the measurement of the time evolution of the drop size distribution in liquid-liquid dispersion in an agitated tank. The effect of droplet size distribution on the impeller speed in water-oil dispersion in agitated vessel was obtained.

Název v anglickém jazyce

In-situ measurement of particle size distribution in an agitated vessel

Popis výsledku anglicky

Agitation of solid-liquid suspension or two immiscible liquids is a frequent operation in chemical and metallurgical industries (suspension/emulsion polymerization, catalytic chemical reaction, hydrometallurgical solvent extraction). The product quality, yield and economy of the processes are significantly affected by a mixing process. Prediction of mean particle/drop size and particle/drop size distribution (PSD) during the agitation is fundamental for emulsification, suspension polymerization, solid particle dispersion or crystallization. The aim of this contribution is to propose a simple method of in-situ measurement of particle size distribution. The particle size measurement is based on an image analysis performed on raw image records. Evaluation method based on the best focused particles with sharp detected boundaries enhanced by the analysis of particle circularity was developed. Precise spherical mono-disperse steel and plastic particles were used to verify accuracy of evaluation method. The method has been proposed for the measurement of the time evolution of the drop size distribution in liquid-liquid dispersion in an agitated tank. The effect of droplet size distribution on the impeller speed in water-oil dispersion in agitated vessel was obtained.

Druh

D - Stať ve sborníku

CEP obor

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OECD FORD obor

20402 - Chemical process engineering

Projekt

<a href="/cs/project/GA16-20175S" target="_blank" >GA16-20175S: Lokální rychlost disipace turbulentní energie v dispersních systémech</a><br>

Návaznosti

P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Rok uplatnění

2017

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Název statě ve sborníku

18th International Conference on Transport & Sedimantation of Solid Particles

ISBN

978-83-7717-269-8

ISSN

1232-3071

e-ISSN

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Počet stran výsledku

7

Strana od-do

177-183

Název nakladatele

Wroclaw University of Environmental And Life Sciences

Místo vydání

Wroclaw

Místo konání akce

Praha

Datum konání akce

11. 9. 2017

Typ akce podle státní příslušnosti

WRD - Celosvětová akce

Kód UT WoS článku

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