Preparation of anorthite ceramics using SPS

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68407700%3A21340%2F21%3A00362700" target="_blank" >RIV/68407700:21340/21:00362700 - isvavai.cz</a>

Nalezeny alternativní kódy

RIV/61389021:_____/21:00544098 RIV/61389005:_____/21:00544098 RIV/00216208:11320/21:10438133

Výsledek na webu

<a href="https://doi.org/10.1016/j.jeurceramsoc.2021.03.004" target="_blank" >https://doi.org/10.1016/j.jeurceramsoc.2021.03.004</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1016/j.jeurceramsoc.2021.03.004" target="_blank" >10.1016/j.jeurceramsoc.2021.03.004</a>

Jazyk výsledku

angličtina

Název v původním jazyce

Preparation of anorthite ceramics using SPS

Popis výsledku v původním jazyce

A mixture of kaolin (92 wt.% of kaolinite) and laboratory-grade CaCO3 was used for anorthite preparation using the spark plasma sintering (SPS) technique. The powder was heated up to the maximum temperature (850 ?C?1100 ?C with a step of 50 ?C, heating rate 50 ?C/min) using the SPS device. The as-prepared samples were compared with a reference sample produced by dry pressing and conventional firing. Rietveld refinement performed on the X-ray diffraction data revealed that before anorthite formation, gehlenite and Ca-feldspar appeared, which gradually transformed into anorthite with increasing temperature. The sample prepared by SPS at 1100 ?C contained 90 wt.% of anorthite, while the anorthite content in the reference sample reached only 47 wt.%. The porosity of the samples prepared by SPS reached significantly lower values compared to that of the reference sample. Therefore, SPS can be considered as a promising technique in the preparation of anorthite ceramics at lower temperatures.

Název v anglickém jazyce

Preparation of anorthite ceramics using SPS

Popis výsledku anglicky

A mixture of kaolin (92 wt.% of kaolinite) and laboratory-grade CaCO3 was used for anorthite preparation using the spark plasma sintering (SPS) technique. The powder was heated up to the maximum temperature (850 ?C?1100 ?C with a step of 50 ?C, heating rate 50 ?C/min) using the SPS device. The as-prepared samples were compared with a reference sample produced by dry pressing and conventional firing. Rietveld refinement performed on the X-ray diffraction data revealed that before anorthite formation, gehlenite and Ca-feldspar appeared, which gradually transformed into anorthite with increasing temperature. The sample prepared by SPS at 1100 ?C contained 90 wt.% of anorthite, while the anorthite content in the reference sample reached only 47 wt.%. The porosity of the samples prepared by SPS reached significantly lower values compared to that of the reference sample. Therefore, SPS can be considered as a promising technique in the preparation of anorthite ceramics at lower temperatures.

Druh

J_imp - Článek v periodiku v databázi Web of Science

CEP obor

—

OECD FORD obor

20504 - Ceramics

Projekt

—

Návaznosti

I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Rok uplatnění

2021

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Název periodika

Journal of the European Ceramic Society

ISSN

0955-2219

e-ISSN

1873-619X

Svazek periodika

41

Číslo periodika v rámci svazku

8

Stát vydavatele periodika

NL - Nizozemsko

Počet stran výsledku

7

Strana od-do

4618-4624

Kód UT WoS článku

000637525500004

EID výsledku v databázi Scopus

2-s2.0-85102771836