Monitoring of vulcanization process using measurement of electrical properties during linear increasing temperature

Kód výsledku v IS VaVaI

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Výsledek na webu

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DOI - Digital Object Identifier

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Jazyk výsledku

angličtina

Název v původním jazyce

Monitoring of vulcanization process using measurement of electrical properties during linear increasing temperature

Popis výsledku v původním jazyce

The article presents the possibilities of diagnostics of irreversible chemical reaction - vulcanization in case of laboratory prepared rubber mixture based on styrene - butadiene (SBR) using measurements of selected physical parameters. Our work is focused on the measurement of current rheologic parameters (torque at defined shear deformation) and selected electrical parameters (DC conductivity) during linear increasing temperature. The individual steps of vulcanization are well identified by means of measurements of rheologic parameters, while significantly affecting the value of the electrical conductivity. The value of the electrical conductivity increases with the increasing of rate of the crossbridging reactions during vulcanization (fig. 1). Therate of the heating affects both types of measurements. When the rate of the heating is increasing the temperature of the beginning of networking step of reactions and also the rate of vulcanization grow. The sensitivity of the both types

Název v anglickém jazyce

Monitoring of vulcanization process using measurement of electrical properties during linear increasing temperature

Popis výsledku anglicky

The article presents the possibilities of diagnostics of irreversible chemical reaction - vulcanization in case of laboratory prepared rubber mixture based on styrene - butadiene (SBR) using measurements of selected physical parameters. Our work is focused on the measurement of current rheologic parameters (torque at defined shear deformation) and selected electrical parameters (DC conductivity) during linear increasing temperature. The individual steps of vulcanization are well identified by means of measurements of rheologic parameters, while significantly affecting the value of the electrical conductivity. The value of the electrical conductivity increases with the increasing of rate of the crossbridging reactions during vulcanization (fig. 1). Therate of the heating affects both types of measurements. When the rate of the heating is increasing the temperature of the beginning of networking step of reactions and also the rate of vulcanization grow. The sensitivity of the both types

Druh

O - Ostatní výsledky

CEP obor

CI - Průmyslová chemie a chemické inženýrství

OECD FORD obor

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Projekt

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Návaznosti

V - Vyzkumna aktivita podporovana z jinych verejnych zdroju

Rok uplatnění

2013

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů