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Powder cohesion and energy to break an avalanche: Can we address surface heterogeneity?

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22310%2F22%3A43925899" target="_blank" >RIV/60461373:22310/22:43925899 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216208:11160/22:10451086

  • Result on the web

    <a href="https://www.sciencedirect.com/science/article/pii/S0378517322007529?via%3Dihub" target="_blank" >https://www.sciencedirect.com/science/article/pii/S0378517322007529?via%3Dihub</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.ijpharm.2022.122198" target="_blank" >10.1016/j.ijpharm.2022.122198</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Powder cohesion and energy to break an avalanche: Can we address surface heterogeneity?

  • Original language description

    The aim of this work is to contribute to the theoretical investigation of cohesive powder surface properties regarding the surface energy both in a qualitative and quantitative way. The relationship between cohesion (shear testing), the energy to break avalanche (avalanche testing) and the surface energy heterogeneity (inverse gas chromatography, IGC) was investigated using binary mixtures of the cohesive drug meloxicam (M) in a range of 5–50% (w/w) and excipients, i.e., alginic acid (AA) and calcium alginate (AC), prepared by mixing and co-milling. A linear relationship was detected between the cohesion and energy to break an avalanche (R2 = 0.633) and the cohesion and specific surface area of the powders (R2 = 0.862). The surface energy heterogeneity measurement at a nominal surface coverage 0.04–0.10 allowed to compare the experimentally estimated work of cohesion (showing the cohesive interaction between the particles) with the theoretical estimation of work of adhesion between a drug and the host carrier. The preference of adhesive forces with the carrier materials was demonstrated in case of M. Better adhesion properties of AA were observed together with the highest dispersive energy, while interestingly, the lowest value of cohesion was also noted for this excipient.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    30104 - Pharmacology and pharmacy

Result continuities

  • Project

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2022

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    International Journal of Pharmaceutics

  • ISSN

    0378-5173

  • e-ISSN

    1873-3476

  • Volume of the periodical

    626

  • Issue of the periodical within the volume

    122198

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    12

  • Pages from-to

    nestrankovano

  • UT code for WoS article

    000869411700009

  • EID of the result in the Scopus database

    2-s2.0-85138837057