Sonochemical synthesis of bismuth(III) nano coordination compound and direct synthesis of Bi2O3 nanoparticles from a bismuth(III) nano coordination compound precursor
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378271%3A_____%2F15%3A00451277" target="_blank" >RIV/68378271:_____/15:00451277 - isvavai.cz</a>
Result on the web
<a href="http://dx.doi.org/10.1007/s10904-015-0231-4" target="_blank" >http://dx.doi.org/10.1007/s10904-015-0231-4</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1007/s10904-015-0231-4" target="_blank" >10.1007/s10904-015-0231-4</a>
Alternative languages
Result language
angličtina
Original language name
Sonochemical synthesis of bismuth(III) nano coordination compound and direct synthesis of Bi2O3 nanoparticles from a bismuth(III) nano coordination compound precursor
Original language description
A new coordination Compound [Bi(L)(NO3)2(ONO2)(CH3OH)] (1) [L: C5H4NCH=NNHCONC5H4] was synthesized by the reaction of Bismuth(III) bromide with the ligand pyridine-2-carbaldehyde isoniazid and characterized by elemental analysis, FT-IR spectroscopy and single-crystal X-ray diffraction. Single crystal X-ray diffraction revealed that the compound 1 is mononuclear complex with Bismuth(III) in a distorted tricapped trigonal prismatic geometry environment of NNO donors of Schiff base ligand, five oxygen atoms of Nitrate molecules and one oxygen atom of methanol molecule. We also synthesized a nano fo rm of the compound 1 by the sonochemical method and delta-Bi2O3 nanoparticles by its calcination.
Czech name
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Czech description
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Classification
Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
BM - Solid-state physics and magnetism
OECD FORD branch
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Result continuities
Project
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Continuities
I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace
Others
Publication year
2015
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Journal of Inorganic and Organometallic Polymers and Materials
ISSN
1574-1443
e-ISSN
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Volume of the periodical
25
Issue of the periodical within the volume
5
Country of publishing house
US - UNITED STATES
Number of pages
7
Pages from-to
1226-1232
UT code for WoS article
000359536800024
EID of the result in the Scopus database
2-s2.0-84938983095