HPLC–MS/MS authentication of the eighteenth century liquorice drug remains and mass spectrometry of selected liquorice-specific compounds
Identifikátory výsledku
Kód výsledku v IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11310%2F24%3A10490784" target="_blank" >RIV/00216208:11310/24:10490784 - isvavai.cz</a>
Výsledek na webu
<a href="https://verso.is.cuni.cz/pub/verso.fpl?fname=obd_publikace_handle&handle=RXfNVfePgv" target="_blank" >https://verso.is.cuni.cz/pub/verso.fpl?fname=obd_publikace_handle&handle=RXfNVfePgv</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1007/s00706-024-03226-z" target="_blank" >10.1007/s00706-024-03226-z</a>
Alternativní jazyky
Jazyk výsledku
angličtina
Název v původním jazyce
HPLC–MS/MS authentication of the eighteenth century liquorice drug remains and mass spectrometry of selected liquorice-specific compounds
Popis výsledku v původním jazyce
In this work, more than 200-year-old historical remains of liquorice root powder and a current liquorice root as a reference material were analyzed by HPLC-MS/MS to confirm the botanical authenticity of the historical material by comparing the results obtained. Combining extraction with different solvents with HPLC-MS/MS successfully identified nine chemotaxonomic markers in the historical material, thus confirming its identity as liquorice. In the current reference material, 32 chemotaxonomic markers of liquorice were successfully identified. Therefore, several liquorice-specific compounds in the historical remains analyzed were shown to have degraded over time. In addition, possible fragmentation mechanisms for five liquorice-specific compounds that have not been previously published in the literature were proposed.
Název v anglickém jazyce
HPLC–MS/MS authentication of the eighteenth century liquorice drug remains and mass spectrometry of selected liquorice-specific compounds
Popis výsledku anglicky
In this work, more than 200-year-old historical remains of liquorice root powder and a current liquorice root as a reference material were analyzed by HPLC-MS/MS to confirm the botanical authenticity of the historical material by comparing the results obtained. Combining extraction with different solvents with HPLC-MS/MS successfully identified nine chemotaxonomic markers in the historical material, thus confirming its identity as liquorice. In the current reference material, 32 chemotaxonomic markers of liquorice were successfully identified. Therefore, several liquorice-specific compounds in the historical remains analyzed were shown to have degraded over time. In addition, possible fragmentation mechanisms for five liquorice-specific compounds that have not been previously published in the literature were proposed.
Klasifikace
Druh
J<sub>imp</sub> - Článek v periodiku v databázi Web of Science
CEP obor
—
OECD FORD obor
10406 - Analytical chemistry
Návaznosti výsledku
Projekt
—
Návaznosti
S - Specificky vyzkum na vysokych skolach<br>I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace
Ostatní
Rok uplatnění
2024
Kód důvěrnosti údajů
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Údaje specifické pro druh výsledku
Název periodika
Monatshefte für Chemie - Chemical Monthly
ISSN
0026-9247
e-ISSN
1434-4475
Svazek periodika
155
Číslo periodika v rámci svazku
8-9
Stát vydavatele periodika
AT - Rakouská republika
Počet stran výsledku
11
Strana od-do
813-823
Kód UT WoS článku
001260372500001
EID výsledku v databázi Scopus
2-s2.0-85197632788