INFLUENCE OF MILLING PARAMETERS ON PARTICLE SIZE AND MICROHARDNESS OF CRYOMILLED AND SPARK PLASMA SINTERED CP Ti

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11320%2F16%3A10335201" target="_blank" >RIV/00216208:11320/16:10335201 - isvavai.cz</a>

Výsledek na webu

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DOI - Digital Object Identifier

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Jazyk výsledku

angličtina

Název v původním jazyce

INFLUENCE OF MILLING PARAMETERS ON PARTICLE SIZE AND MICROHARDNESS OF CRYOMILLED AND SPARK PLASMA SINTERED CP Ti

Popis výsledku v původním jazyce

Ultra-fine grained (UFG) materials are in the spotlight because of their enhanced mechanical properties. UFG material can be prepared by bottom-up process consisting of agglomeration of nano-particles or by top-down process of severe plastic deformation (SPD) In this study, Ti Grade 2 powder underwent attritor milling in liquid nitrogen (LN) and argon (LAr) and was consequently consolidated via spark plasma sintering (SPS). The influence of milling liquid (LN vs. LAr), of milling balls material (stainless steel vs. tungsten carbide) and of other milling parameters (e.g. speed, duration) on size and shape of powder particles, chemical contamination and microhardness was investigated. Particle size reduction was generally not observed, while their morphology changed significantly due to simultaneous disintegration and intensive cold welding during the milling process. Using LN as a cooling medium resulted in very high nitrogen content (up to 3 wt.%), and consequent embrittlement and hardening with microhardness values attaining 800 HV. LAr seems to be more suitable for milling of titanium, but a process control agent (stearic acid) must be added to prevent excessive cold welding. Microhardness of material without nitrogen contamination rose from original 178 HV to 200-300 HV range, depending on milling efficiency.

Název v anglickém jazyce

INFLUENCE OF MILLING PARAMETERS ON PARTICLE SIZE AND MICROHARDNESS OF CRYOMILLED AND SPARK PLASMA SINTERED CP Ti

Popis výsledku anglicky

Ultra-fine grained (UFG) materials are in the spotlight because of their enhanced mechanical properties. UFG material can be prepared by bottom-up process consisting of agglomeration of nano-particles or by top-down process of severe plastic deformation (SPD) In this study, Ti Grade 2 powder underwent attritor milling in liquid nitrogen (LN) and argon (LAr) and was consequently consolidated via spark plasma sintering (SPS). The influence of milling liquid (LN vs. LAr), of milling balls material (stainless steel vs. tungsten carbide) and of other milling parameters (e.g. speed, duration) on size and shape of powder particles, chemical contamination and microhardness was investigated. Particle size reduction was generally not observed, while their morphology changed significantly due to simultaneous disintegration and intensive cold welding during the milling process. Using LN as a cooling medium resulted in very high nitrogen content (up to 3 wt.%), and consequent embrittlement and hardening with microhardness values attaining 800 HV. LAr seems to be more suitable for milling of titanium, but a process control agent (stearic acid) must be added to prevent excessive cold welding. Microhardness of material without nitrogen contamination rose from original 178 HV to 200-300 HV range, depending on milling efficiency.

Druh

D - Stať ve sborníku

CEP obor

BM - Fyzika pevných látek a magnetismus

OECD FORD obor

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Projekt

<a href="/cs/project/GA15-15609S" target="_blank" >GA15-15609S: Ultra-jemnozrnné a nanokrystalické kovové materiály s vysokou pevností připravené slinovaním pulzním elektrickým proudem</a><br>

Návaznosti

P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Rok uplatnění

2016

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Název statě ve sborníku

METAL 2016: 25TH ANNIVERSARY INTERNATIONAL CONFERENCE ON METALLURGY AND MATERIALS

ISBN

978-80-87294-67-3

ISSN

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e-ISSN

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Počet stran výsledku

6

Strana od-do

1439-1444

Název nakladatele

TANGER LTD

Místo vydání

SLEZSKA

Místo konání akce

Brno

Datum konání akce

25. 5. 2016

Typ akce podle státní příslušnosti

WRD - Celosvětová akce

Kód UT WoS článku

000391251200235