Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry
Identifikátory výsledku
Kód výsledku v IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216224%3A14310%2F09%3A00036101" target="_blank" >RIV/00216224:14310/09:00036101 - isvavai.cz</a>
Výsledek na webu
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DOI - Digital Object Identifier
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Alternativní jazyky
Jazyk výsledku
angličtina
Název v původním jazyce
Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry
Popis výsledku v původním jazyce
Development of LC/MS/MS method for analysing polycyclic aromatic nitrogen hydrocarbons (PANHs) in soil samples is presented. Optimisation of individual chromatographic/mass spectrometric conditions was made in order to obtain a method for the determination of 15 PANHs content in an organic extract from the soil. Detection limits (LOD) in the range of 0.3 to 15 pg per injection were 15 obtained for individual PANHs. LC/MS/MS method has a lower LOD value compared to LC/DAD/FLD methods in general. Developed LC/MS/MS method was used for determination of PANHs content in soil samples collected in contaminated areas of the southeast region of the Czech Republic. Highest concentrations of PANHs have been found in the samples collected in the immediate vicinity of the industrial basin. Concentrations of the contaminants in samples collected in surrounding villages were higher compared to the sample collected in clean area of the Czech Republic.
Název v anglickém jazyce
Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry
Popis výsledku anglicky
Development of LC/MS/MS method for analysing polycyclic aromatic nitrogen hydrocarbons (PANHs) in soil samples is presented. Optimisation of individual chromatographic/mass spectrometric conditions was made in order to obtain a method for the determination of 15 PANHs content in an organic extract from the soil. Detection limits (LOD) in the range of 0.3 to 15 pg per injection were 15 obtained for individual PANHs. LC/MS/MS method has a lower LOD value compared to LC/DAD/FLD methods in general. Developed LC/MS/MS method was used for determination of PANHs content in soil samples collected in contaminated areas of the southeast region of the Czech Republic. Highest concentrations of PANHs have been found in the samples collected in the immediate vicinity of the industrial basin. Concentrations of the contaminants in samples collected in surrounding villages were higher compared to the sample collected in clean area of the Czech Republic.
Klasifikace
Druh
J<sub>x</sub> - Nezařazeno - Článek v odborném periodiku (Jimp, Jsc a Jost)
CEP obor
CB - Analytická chemie, separace
OECD FORD obor
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Návaznosti výsledku
Projekt
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Návaznosti
Z - Vyzkumny zamer (s odkazem do CEZ)<br>S - Specificky vyzkum na vysokych skolach
Ostatní
Rok uplatnění
2009
Kód důvěrnosti údajů
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Údaje specifické pro druh výsledku
Název periodika
International Journal of Environmental analytical cemistry
ISSN
0306-7319
e-ISSN
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Svazek periodika
Vol. 89
Číslo periodika v rámci svazku
No. 3
Stát vydavatele periodika
GB - Spojené království Velké Británie a Severního Irska
Počet stran výsledku
15
Strana od-do
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Kód UT WoS článku
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EID výsledku v databázi Scopus
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