Plasma Chemical Reduction of Model Corrosion Brass Layer Prepared in Soil

Kód výsledku v IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216305%3A26310%2F16%3APU120317" target="_blank" >RIV/00216305:26310/16:PU120317 - isvavai.cz</a>

Výsledek na webu

<a href="http://dx.doi.org/10.1051/epjap/2016150588" target="_blank" >http://dx.doi.org/10.1051/epjap/2016150588</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1051/epjap/2016150588" target="_blank" >10.1051/epjap/2016150588</a>

Jazyk výsledku

angličtina

Název v původním jazyce

Plasma Chemical Reduction of Model Corrosion Brass Layer Prepared in Soil

Popis výsledku v původním jazyce

Samples corroded naturally more than two years in the soil in the vertical and horizontal positions, so the corrosion layers were the most similar to the corrosion layer of original archaeological artifacts. The samples were treated in the low pressure (150 Pa) in a hydrogen-argon gas mixture at mass flows of 30 sccm for hydrogen and 20 sccm for argon for 90 minutes. 13 samples were treated. The plasma power was 100, 200, 300, and 400 W in continuous and pulsed mode. Maximum sample temperature was set at 120 °C. The whole process was monitored by optical emission spectroscopy and the obtained data were used to calculate the relative intensity of OH radicals and rotational temperature. The results showed that the higher power had the greater maximum intensity of the OH radicals and rapidly degraded the corrosion layer. Corrosion layer was not completely removed during the reduction, but due to the reactions which occur in the plasma corrosion layer became brittle and after plasma chemical treatment can be removed easily.

Název v anglickém jazyce

Plasma Chemical Reduction of Model Corrosion Brass Layer Prepared in Soil

Popis výsledku anglicky

Samples corroded naturally more than two years in the soil in the vertical and horizontal positions, so the corrosion layers were the most similar to the corrosion layer of original archaeological artifacts. The samples were treated in the low pressure (150 Pa) in a hydrogen-argon gas mixture at mass flows of 30 sccm for hydrogen and 20 sccm for argon for 90 minutes. 13 samples were treated. The plasma power was 100, 200, 300, and 400 W in continuous and pulsed mode. Maximum sample temperature was set at 120 °C. The whole process was monitored by optical emission spectroscopy and the obtained data were used to calculate the relative intensity of OH radicals and rotational temperature. The results showed that the higher power had the greater maximum intensity of the OH radicals and rapidly degraded the corrosion layer. Corrosion layer was not completely removed during the reduction, but due to the reactions which occur in the plasma corrosion layer became brittle and after plasma chemical treatment can be removed easily.

Druh

J_imp - Článek v periodiku v databázi Web of Science

CEP obor

—

OECD FORD obor

60102 - Archaeology

Projekt

<a href="/cs/project/DF11P01OVV004" target="_blank" >DF11P01OVV004: Plazmochemické procesy a technologie pro konzervaci kovových archeologických předmětů</a><br>

Návaznosti

P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Rok uplatnění

2016

Kód důvěrnosti údajů

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Název periodika

EUROPEAN PHYSICAL JOURNAL-APPLIED PHYSICS

ISSN

1286-0042

e-ISSN

1286-0050

Svazek periodika

75

Číslo periodika v rámci svazku

2

Stát vydavatele periodika

FR - Francouzská republika

Počet stran výsledku

6

Strana od-do

„24717--1“-„24717-6“

Kód UT WoS článku

000380828500017

EID výsledku v databázi Scopus

2-s2.0-84981337921